Laboratory report of GCMS analysis for sample AE10064 conducted on May 23, 2002, showing surrogate recovery data.
NYC-WTC_000023718–000023727Folder label: “GCMS X 5/9/02 A 5/20/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File C:\HPCHEM\1\DATA\MAY0302\10064.D Vial: 37 Acq On 5 May 2002 3:18 am Operator: Sample GC/MS SCAN 4/26 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L
Peak Number 1 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1
R.T. EstConc Area Relative to ISTD R.T. 8.16 14.26 ug/1 983472 1,4-Dichlorobenzene-d4 12.19 Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 2-Pentanone, 4-hydroxy-4-me thy 1- 116 C6H1202 000123-42-2 50 2 3 -Hydroxy- 2-pentanone 102 C5H10O2 003142-66-3 9 3 CH2=CHCH2C (0) OCH3 100 C5H802 003724-55-8 9 4 Acetone 58 C3H6O 000067-64-1 7 Abundance Scan 340 (8.159 min): 10064.D (-) m/z 43.05 100.00%| 43
5000 59
101 7 80 8.00 8.20 8.40 8.60 .......................38 +53+ 'I I ' 1 ' 69 77 83 , | ■ i ' ‘ ‘ ■ i ‘ ■ ■ ■ i ' 1 1 1 1 1 1 1 1 1 1 m/z 59.10 43.97% miz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #64275:2-Pentanone, 4-hydroxy-4-methyl- 4)3
5000 59 7 80 8.00 8.20 8.40 8.60 m/z 58.10 16.39%| 15 31 — 83 101 | I ' I1' + ■■ ■ l ' ''I i ■ ■ ■ ■ i ' ' ' 1 I ''' ' ' i ' ' 1 1 1 1 1 1 1 1 1 miz—> 10 20 30 40 50 60 70 80 90 100 110 Abundance #1691:3-Hydroxy-2-pentanone 31 59
7.80 8.00 8.20 8.40 8.60 5000 m/z 101.15 13.90%| 45 15 . 66 73 84 102 ' ■ i ‘ ' 1 1 1 1 1 1 I1 1 1 1 1 1 ■ ■ i ' ' 1 I ' 1 1 1 i ' ■ ■ ' i ■ 1 ' ■ i ' 1 1 1 i 1 1 ' ' 1 1 miz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #1448: CH2=CHCH2C(O)OCH3 43 7 80 8.00 8.20 8.40 8.60 m/Z 41.05 7.01% 5000
m/z—> —...... .1 10 20 30 40 . 5. 72. 50 60 70 PPPP— 80 90 100 100 110 TrTmOrTTT 7.80 8.00 8.20 8.40 8.60
10064.D GCMS0501.M Tue May 07 12:00:47 2002 Page 1
NYC-WTC_000023723
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NYC-WTC_000025533
Fragmented GCMS scan data page showing tentative identification of compounds and surrogate recovery for sample AE10812.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000022953
GCMS calibration table and instrument data for TCLP analysis recorded on May 5-7, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000022930
GCMS calibration table and instrument data for TCLP analysis recorded on May 5-7, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023195
Calibration table listing response factors for deuterated standards used in TCLP analysis on May 5, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000013117
Calibration table listing response factors for deuterated standards and target compounds used in gas chromatography-mass spectrometry analysis.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000045452
Technical document displaying GCMS calibration data and compound retention times for sample AE09391 processed in early May 2002.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000045507
Technical document displaying GCMS calibration data and compound retention times for sample AE09449 processed in early May 2002.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000046294
Laboratory report showing GCMS calibration data for sample AE09585 generated on May 4-6, 2002.
1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000046332
Laboratory report showing GCMS calibration data for sample AE09587 generated on May 4-6, 2002.
1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000013146
Calibration table listing response factors for deuterated standards and target compounds used in gas chromatography-mass spectrometry analysis.
1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000046351
Laboratory report showing GCMS calibration data for sample AE09334 generated on April 25-26, 2002.
1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000011494
Instrument output displaying calibration data and surrogate recovery results for sample AE03381.
1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000023646
Department of Environmental Protection administrative record sheet for World Trade Center site activities dated May 2002.
Filed in the same folder
NYC-WTC_000023647
Technical data file header page from a GCMS analysis run associated with the World Trade Center site in May 2002.
Filed in the same folder
NYC-WTC_000023649
Laboratory report showing GC/MS blank analysis for sample AE09676 with non-detect results for volatile organic compounds.
Filed in the same folder
NYC-WTC_000023662
Laboratory report showing GC/MS calibration data for volatile organic compounds analyzed on May 20-21, 2002.
Filed in the same folder
NYC-WTC_000023666
Laboratory report showing GC/MS reference analysis for sample AE09676 with quantitative results for volatile organic compounds.
Filed in the same folder