GCMS unknown compound analysis, sample AE05515, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\APR0102\5515.D Vial: 6 Acq On 1 Apr 2002 4:11 pm Operator: Sample gc/ms scan 3/11 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P '

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 3 Butane, 2,3-dichloro-2-methyl- Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T.

7.76 0.75 ug/1 127228 1,4-Dichlorobenzene-d4 12.25

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Butane, 2,3-dichloro-2-methyl- 140 C5H10C12 000507-45-^3 2 1-Propene, 2-chloro- 76 C3H5C1 000557-98-2^- 3 Propane, 2-chloro-2-nitro- 123 C3H6C1NO2 000594-71-8 9 4 Propane, 1,1-dichloro- 112 C3H6C12 000078-99-9 9 Abundance Scan 296 (7.760 min): 5515.D (-) m/z 76.95 100.00% 7|7

41 ma 69 ' I ' ' ' I ' ’ 7T7 , . , , I r

MV I 89 [I 84 T., , / 1^5 I ■......... 7.40 m/ 2 7.60 41.05 7.80 8.00 59.8^% 8.20

____ 20____ 30 Abundance 40 50 60 70 80 90 100 #7245: Butane, 2,3-dichloro-2-m"ethyr 110 120 130 ft 7|7

5000 ri 1 1 I 7.40 7.60 7.80 8.00 8.20 69 m/ z 75.90 27 39.33% 53 63

fn/z-> 20 I 30 35 40 . I. I i-YT'^r-r-ryT-^r-T-r^ 50 60 70 80 € 90 100 89 . 110 J- 120 125. , 130 Abundance #62597: 1-Propene. 2-chloro- 41

7.40 7.60 7.80 8.00 8.20 7.6 5000 m/z 69.10 31.42%

31 ,! . 49 61 I

'U ' I ' ' ' ' I ' m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #3996: Propane. '2-chloro-2-nitro^ 717 7.40 Z:60 t80 8t0 8^ m/z 78.95 28.84% 5000

49 61 ' I ................................ ...... T)/Z-> 20 30 40 50 60 70 80 90 100 110 120 130 7.40 7.60 7.80 8.00 8.20

5515.D GCMS0403.M . Thu Apr 04 13:52:59 2002 Page 3

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