GCMS analysis results for sample AE04129, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\MAR2202\4129.D Vial: 25 Acq On : 23 Mar 2002 7:44 pm Operator: Sample : gc/ms scan 2/25 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 7 Butane, 1,3-dichloro-3-methyl- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

9.71 7.70 ug/1 890129 1,4-Dichlorobenzene-d4 12.26

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Butane, 1,3 -dichloro-3 -methyl - 140 C5H10C12 000624-96-4 36 2 1-Pentene, 3-bromo-4-methyl- 162 C6HllBr 000815-47-4 27 3 Butane, 2,3-dichloro-2-methyl- 140 C5H10C12 000507-45-9 22 4 2-Butene, 1-bromo-3-methyl- 148 C5H9Br _______ 000870-63-3 16 Abundance Scan 508 (9.712 min): 4129.D (-) m/z 41. 05 100.00% 41 69 105

77 5000 53 - 151

m/z-> ' I" " I" 14 20_ 30 40 |l 614 R I., 121 135 171 || 111 ■ ■1 ■ i ■ ■ ■ ■ i ■■■• ■ i11 ■ ■ i1 • • * । * * • ’1* ■ ■ ■ । 50 60 70 80 90 100 110 120 130 140 150 160 170 9.40 9.60 9.80 10.00 m/z 104.95 ' 96.79% Abundance #7246: Butane, 1,3-dichloro-3-methyl- 41 69 77 5000 TTI 27 9.40 9.60 9.80 10.00 53 105 89 m/z 69.10 91.86% II TH I ■1 ■ ■ i ■ “ ■ i ■ ■ • ■ i ■ “ ' i ■ • ■ ■ i ■ ■ ■ ■ i mz—s 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 Abundance :7 itpe 3-bror,:-4 methyl- 41 69 ----- 9.40 9.60 9.80 10.00 5000 m/z 76.95 52.02% 27 53 _______________ _________ 106 ________ 148________ ‘ i “ " i “ • ■ i “ “ i ‘1 ■ ■ i “ ■ • i ■ ■ " i1 ■1' i' • ■' i “ “ I' •1 • i' " ‘ i1 • ■ ■ i “ '11 “ “ i ‘ " i' “ ‘ i m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170__ Abundance #7245: Butane, 2,3-dichloro-2-methyl- ■ ■ i ■ 1 ■ 1 I ‘ 1 1 1 1 1 1 1 1 I 1 1 11 I 77 9.40 9.60 9.80 10.00 m/z 39.0,5 33.72% ... ..................... 5000 69 ! 27 | 35 53 89 105 . 1...... 1 I. 125 ’ I ‘ ” 11 ‘ •11' ■i1 ‘ ■ ■ i ■ ■ i ■ t । .... j । i . q rrr. ,r j rrr. | m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 9.40 9.60 9.80 10.00 _

4129.D GCMS0308.M Wed Mar 27 10:06:41 2002 Page 7

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