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GCMS analysis results for sample AE04129, April 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of environmental sample AE04129 conducted on April 1, 2002.

NYC-WTC_000011800–000011816

Folder label: “GCMS X 2/25/02 A 3/23/02

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Scanned page image, NYC-WTC_000011814
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\MAR2202\4129.D Vial: 25 Acq On : 23 Mar 2002 7:44 pm Operator: Sample : gc/ms scan 2/25 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 8 1,5-Pentanediol Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T.

10.02 0.61 ug/1 70086 1,4-Dichlorobenzene-d4 12.26

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1,5-Pentanediol/ 104 C5H12O2 000111-29-5 9 2 2-Butanone, 3-methoxy-3-methyl- 116 C6H1202 036687-98-6 9 3 3,4-Dimethyl/5-hexen- 3-ol 128 C8H160 000000-00-0 9 4 Octanal, 7-methoxy- 3,7-dimethyl- 186 C11H22O2__ _____ 003613-30-7 9 Abundance — f Scan 541 (10.015 min): 4129.D (-) m/z 73.00 * 100.00% 73

5000 43 57 139 ..... ............. / 151 9.60 9.80 10.00 10.20 10.40 1. 59.1 Iguni r’ +r 85 93 m/z 43.00 41.04% m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #1923:1,5-Pentanediol 311 56 . .. ■

5000 44 68 9.60 9.80 10.00 10.20 10.40 m/z 138.95 36.42% I ‘1 t 1111 TT-J-TT 13 1‘tt-1r‘‘11-r1‘1111111111112231101TF3IITOO ‘I1" miz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance $3263 2-Butaut j te kema 73

43 9.60 9.80 10.00 10.20 10.40 5000 m/z 57.00 36.19%

57 85 ’111’’1/’/1111111111-5331111120119321193O203I—CIIOIrIIIITCTOIGI7Tr 101 miz-> 20__ 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #5018:3,4-Dimethyl-5-hexen-3-ol 73 9.60 9.80 10.00 10.20 10X0 m/z 136." 35.19% 43 5000 55

27

miz-? J TTTH 81 99 .......,..........11 .. 1 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 ■ i' ■ 1' i ■■ i' ■ ‘ • i1 '1' I"''11!1 1111111 ' 11'1' I' 9.60 9.80 10.00 10.20 10.40

4129.D GCMS0308.M Wed Mar 27 10:06:45 2002 Page 8

NYC-WTC_000011814

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NYC-WTC_000011814Source: NYC Law Department, mirrored locally

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