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GCMS analysis results for sample AE02645, Mar 15, 2002

Machine-extracted title · confidence 90%

Laboratory report listing unknown compounds and surrogate recovery data for sample AE02645.

NYC-WTC_000005415–000005434

Folder label: “GCMS X 2/5/02 A 3/7/02

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Scanned page image, NYC-WTC_000005422
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document Library Search Compound Report

Data File C:\HPCHEM\1\DATA\MAR0 7 02\2645.D Vial: 18 Acq On 8 Mar 2002 6:27 am Operator: Sample gc/ms scan 2/5 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 3-Pentanol, 3-methyl- Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

8.19 0.56 ug/1 72698 1,4-Dichlorobenzene-d4 12.30

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Pentanol,/ 3-methyl- 102 C6H140 000077-74-7 12 2 N-Ethylformamide 73 C3H7NO 000627-45-2 9 3 Pentadecylamine 227 C15H33N 002570-26-5 9 4 Butane, 2-methoxy-2-methyl- 102 C6H140 000994-05-8 9 Abundance • Scan 343 (8.193 min): 2645.D (-) m/ z 73.00 100.00% 73

5000 43 ............ 1 ,...............

M 1 55 i 37 103 7.80 8.00 8.20 8.40 8.60 ........... . ip'..Al ' i ■ i ■ i ‘ 1 ' ' i ■ ' ' ' i ' ' ' 1 i ' ' ' ■ i ' ' 1 ' i ' ' m/ z 43.05 * 43.94% m/z-> 20 40 60 80 100 120 140 160 180 200 220 Abundance #63572: 3-Pentanol, 3-methyl- 73

AA 5000 55 7.80 8.00 8.20___ 8.40 8.60 45 87 m/z 41.05 17.52% 27 1 1 ' I i I । ।11 ' ' l । ' m/Z=?20 .40 60 80 100 120 140 160 180 200 220 Abundance 30 73 7.80 8.00 8.20 8.40 8.60 5000 m/ z 70.10 12.65% 44 58 15 miz-> 20 40 60 80 100 120 140 160 180 200 220 Abundance #29384: Pentadecylamine 30 7.80 8.00 8.20 8.40 8.60

5000 m/z "7 T 44 Il 57 69 86 100 184 198 212 227 ■ 1 I ' ' ' 1 i 1 ' ' 1 i ' ' 1 ' i 1 ' ' ' I ' ' ■ ■ i ' ' ' 1 i ■ ■ ■ ' i r ' ' ■ i 1 ‘ ■ i ' ' ‘ ' i 1 ' 1 n/z-> 20 40 60 80 100 120 140 160 180 200 220 7.80 8.00 8.20 8.40 8.60

2645.D GCMS0208.M Wed Mar 13 14:54:03 2002 Page 1

NYC-WTC_000005422

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NYC-WTC_000005422Source: NYC Law Department, mirrored locally

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