GCMS calibration results for sample AE03076, March 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\MAR0102\3076.D Vial: 28 Acq On 2 Mar 2002 12:51 pm Operator: Sample gc/ms scan 2/12 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 3-Pentanol, 3-methyl- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

8.20 0.62 ug/1 69214 1,4-Dichlorobenzene-d4 12.32

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Pentanol, 3-methyl- 102 C6H140 000077-74-7 28 2 N-Ethylformamide 73 C3H7NO 000627-45-2 9 3 Silane, tetramethyl- 88 C4H12S1 000075-76-3 9 4 Butane, 2-methoxy-2-methyl-... .. 102 C6H140 000994-05-8 9 Abundance Scan 344 (8.197 min): 3076.D (-) m/z 73.00 100.00% 73

5000 43 -r-j-rT-T-T-f-r tr 87 103 7.80 8.00 8.20 8.40 8.60 । 1, I 49 5.5, . । | , ■ ■ i ■ ■ ‘ ■ i • ■ 1 ■ t ‘ ■ ■ atln—a - I '•■'■'''I ■ ■ ■ ■ 'I'■ 1 1 ' 1 1 1 11 1 ■ ■ > ■ l । r m/z 43.05 27.29% m/z~> 10 20 30 40 50 60 70 80 90 100 110 Abundance #63573: 3-Pentanol, 3-methyl- 73

5000 7.80 8.00 8.20 8.40 8.60 55 m/z 44.95 11.71% 45 87 27 | 39, I 1 ■ 11* m/z-> 10 ‘ ‘ 20 ‘ 30 ‘ ‘ 40 50 60 70 80 90 100 110 Abundance 200: f - :foon . 30 73 7.80 8.00 8.20 8.40 8.60 5000 m/z 41.05 11.07% 44 58

15

m/z-> Abundance IIPTPTT ■ • i ' ■ ■ 1 i ■ ‘ ■ i ■ • ‘ 1 i 1 ' • ' i ‘ 10 20 30 40 50 60 70 ;#62932: Silane, tetramethyl- 80 90

73 ■ i ■ ■ ' ■ i ' 100 110 ...... sl 1 i 1 1 1 1 ■ i ■ 1 ■ • i '11 ” । 7.80 8.00 8.20 8.40 8.60 m/z 71.00 7.36% 5000

miz-> ■ ■ I ‘ 15 • l * ‘

10 20 ‘ |

30 ‘ 45 • j ,I ,1

40 50 ’ i' ‘ ■59 ! « • | 53 1' | i r ■ i ■ J ■ i

60 70 ■ • i ‘ 80 88 • 1 i ■ ‘ 90 ‘ i 1 ‘ 100 ‘ i • 110 ■ i • ■ ■ 1 i ' ' 7.80 8.00 J.... 8.20 8.40 8.60

3076.D GCMS0208.M Tue Mar 05 14:45:45 2002 Page 1

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