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← Document results/DEP Box 14/GCMS X 2/12/02 A 3/19/02
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GCMS calibration results for sample AE03076, March 2002

Machine-extracted title · confidence 100%

Laboratory report showing GC/MS calibration data and surrogate recovery for sample AE03076 on March 22, 2002.

NYC-WTC_000011105–000011112

Folder label: “GCMS X 2/12/02 A 3/19/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\MAR0102\3 0 76.D Vial: 28 Acq On 2 Mar 2002 12:51 pm Operator: Sample gc/ms scan 2/12 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Antipyrine Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

25.85 0.27 ug/1 42729 Phenanthrene-dl0 25.71

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Antipyrine 188 C11H12N2O 000060-80-0 40 2 Pentacyclo[8.4.0.0(3,7).0(4,14).0(6 188 C14H20 000000-00-0 36 3 Anthracene-dlO- 188 C14D10 001719-06-8 32 4 Benzene, 1-(1-cyclohexen-l-yl)-4-me 188 C13H160 020758-60-5 28 Abundance Scan 2267 (25.851 min): 3076.D (-) m/ Z 188710 100.00% 188

5000 94 54 - 80 160 25.60 25.80 26.00 26.20 i 66 .J I “ । ■ 11 H '11 • i “ ।11 ■ ■ • ■ i1 ‘ ■--m* m/z 94.00 19.56% mfe-> 50 60 70 80__ 90 100 110 120 130 140 150 160 170 180 190 Abundance #19872: Antipyrine 188 96 ..................... ......................... 5000 77 56 25.60 25.80 26.00 26.20 105 m/z 189.10 18.36% 84 159 173 '■ II ” ■ i ■ ■' * i ■ TTImmupuupmnmmummugmtpt 1’3 miz-> 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance S9: Fanoyeol8.4.0,0/3,7)014.14/010 : onm 188 ......... 25.60 25.80 26.00 26.20 5000 m/z 80.00 10.88% 79 op 106 117 131 159 173 miz-s 50"6o" 70 “ 80 “ 90 ‘ 100 ilO 120 130 UP 150 160 170 180 -190* Abundance #19957: Anthracene-d10- 188 25.60 25.80 26.00 26.20 m/z 159.95 10.01% 5000-

0) 66 T 94 160 T’’ ■ ■ i • ■ r ' i1'1 ■ ■ r1 1 m/z~> 50 60 70 80 90 100 110 J 20 130 140 150 160 170 180 190 25.60 25.80 26.00 26.20

3076.D GCMS0208.M Tue Mar 05 14:45:50 2002 Page 2

NYC-WTC_000011111

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NYC-WTC_000011111Source: NYC Law Department, mirrored locally

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