GCMS calibration table for TCLP method, March 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\MAR0102\3383.D Vial: 47 Acq On 3 Mar 2002 9:36 am Operator: Sample gc/ms scan 2/4 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 2 Antipyrine Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

25.86 0.40 ug/1 92105 Phenanthrene-dl0 25.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Antipyrine / 188 C11H12N2O 000060-80-0 59 2 - (4-Tolyl) -3-ymethyl-pyrazol-S-one 188 C11H12N2O 035496-19-6 53 3 Benzene, 1-(1-cyclohexen-1-y1) -4-me 188 C13H160 020758-60-5 38 4 Anthracene-^10-________ _____ 188 C14D10 001719-06-8 38 Abundance T Scan 2267 (25.857 min): 3383.D(-) m/z 188.1O100.00% 4 4 188 5000 _ . ......... 42 54 66 80 92 146 160 , ,i 25.60 25.80 26.00 26.20 m/z~> mhmmmmmmmpmmmmmmmmm 40 _50 60 70 80 90 100 110 120 130 140 150160 170 180 190 m/z 80.05 12.55% Abundance #19872: Antipyrine ‘ "" i ...... .. 188 96 5000 77 56 25*60 25.80 26.00 26.20 105 m/z 189.10 11.93% 159 173 ■ ■ ■ । ■ ■ ■' । • -rp-n-rp- m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance 1965 (—To; •: 188 91 • ■ i ■ 1 I ‘ ■ i ' ■ 25.60 25.80 26.00 26.20 105 5000 m/z 187.20 10.07% 119 65 78 146 TI’15t5n0——90d000a000tuuumu]upppmigr m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19943: Benzene, 1-(1-cyclohexen-1-yl)-4-methoxy- 188 25.60 25.80 26.00 26.20 m/z 160.05 8.00% 5000- 160

121 129 145 173 . ....................................... “i* i ‘ ‘ i “' * ‘ i •• ‘ i '“I “ ■* i 11 1 11 * ....... ’1,*»....• I 1 ’ “ * 1111 1 ‘ 111111 * i »1 m/z-> 40 50 60 70 80 90 100 1 io 120 130 140 150 160 170 180 190 25.60 25.80 26.00 26.20

3383.D GCMS0208.M Mon Mar 25 12:23:28 2002 Page 2

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