GCMS analysis results, sample AE12151, June 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\HPCHEM\l\DATA\MAY3102\12151.D Vial: 8 Acq On : 31 May 2002 6:52 pm Operator: Morgan Sample : gc/ms scan 5/29 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0531.M (RTE Integrator) . Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Phenanthrene-diO Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T. 25.57 0.48 ug/1 44174 Phenanthrene-dl0 25.43 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Phenanthrene-diO 188 C14D10 001517-22-2 64 2 Anthracene-d10- 188 C14D10 001719-06-8 40 3 Antipyrine 188 C11H12N2O 000060-80-0 9 4 3H-Pyrazol-3-one, 2>4-dihydro-4,4-d 188 C11H12N2O 017694-06-3 9 Abundance Scan 2236 (25.569 min): 12151 .D (-) m/z 188.10 100.00% 188

5000

80 94 ■ i ■ • 1 1 i ■ ■ ■ ■ i ■

160 25.20 25.40 25.60 25.80 49 66 11111011111111101111131111371 m/z 94.05 18.44% mz—> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19958: Phenanthrene-d10 188

5000 25.20 25.40 25.60 25.80 m/z 189.10 15.77% 66 80 94 160

mfz—> i" " i “ ■ ■ i I . I , I . . . . |t- . . I I . I 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 mmgpgl] —.. W... Abundance #19957: Anthracene-d10- 188

25.20 25.40 25.60 25.80 ‘ ‘ ‘ ‘ 5000 m/z 80.00 14.89%

--- 66 80 94 160 I . i । ■ i । 11 m i । 11 i i| i ! i i 11 i 11 | 1111 11 i 11 । r I’T miz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #69177: Antipyrine 188 25.20 25.40 25.60 25.80 96 m/z 184.10 11.36% 77 5000 56 31 105

m/z—> 46 mH ‘ I' ■ " I ‘ XU |......... 145 159.173 ... i"1 ‘i“i""i"I "•'i• ■ ■'i ■ ■ “i■"• i■ ■111 ■■ ■■ 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 25.20 25.40 25.60 25.80

12151.D GCMS0531.M Mon Jun 03 09:34:45 2002 Page 2

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