GCMS blank analysis results, Sample AE04417, Mar 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\MAR2102\LB.D Vial: 3 Acq On : 21 Mar 2002 1:15 pm Operator: Sample : gc/ms scan 3/1 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 3 Phenanthrene-diO Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

25.80 0.26 ug/1 56123 Phenanthrene-dl0 25.66

Hit# of Tentative ID5 MW MolForm CAS# Qual

1 Phenanthren ZdlO 75 188 C14D10 001517-22-2 93 2 Anthracene -d10- 188 C14D10 001719-06-8 90 3 Antipyrine 188 C11H12N2O 000060-80-0 42 4 Cyclohexanone, phenylhydrazone 188 C12H16N2 000946-82-7 36 Abundance t Scan 2260 (25.795 min): LB.D (-) m/z 188.10 100.00% 188

5000

80 94" I 1 " ' 1 1 1 1 1 I “ 1 1 I 1 1 1 1 I " 1 1 158 । 25.40 25.60 25.80 26.00 26.20 miz-> 42 66 ■ ■ ■ i1 ■ " i ■ ■ ■ ■ 1 ■11 ■ 1 ■ ■ ' 11 1 ‘

40 50 60 70 ‘ T'r 80 90 100 110 120 130 140 150 160 170 180 190 + ri i i । > ri i । l-|*l L m/z 189.10 17.96% Abundance #19958: Phenanthrene-d10 188

5000 25.40 25.60 25.80 ‘26.00 26.20 % m/z 18 .10 14.28%

miz-s 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance 41 9957; Anthracene-d10 188 - 25.40 25.60 25.80 26.00 26.20 5000 m/z 80.05 14.25%

66 80 94 160 mmmpe ‘ i1 ■ । ■ “ ■ i ‘ ■■ • i • “ 1111'11 “ “ 1111' I " 111111 MT 111111 is 1111 m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 ................................ Abundance #19872: Antipyrine 188 25.40 25.60 25.80 26.00 26.20 96 m/ z 9 .00 11.96% 5000 77 56 105 || 159 173 j JI ’ “ ’ I ’ ‘ mH ■'i ‘1" ■ i ■ “111 “ 11 “11111 “ I " “'11' “ I “ " I “ ‘188 IL .......... / m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 25.40 25.60 25.80 26.00 26.20

LB.D GCMS0308.M Fri Mar 22 09:47:34 2002 Page 3

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