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GCMS analysis results for sample AE04024, Mar 15 2002

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Laboratory report documenting GCMS analysis of sample AE04024 conducted on March 15, 2002.

NYC-WTC_000038302–000038313

Folder label: “GCMS X 2/22/02 A 2/24/02

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Scanned page image, NYC-WTC_000038312
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\FEB2102\4024.D Vial: 79 Acq On : 24 Feb 2002 11:45 pm Operator: Sample : gc/ms scan 2/22 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 4 Phenanthrene-diO Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

25.87 0.23 ug/1 20533 Phenanthrene-diO 25.73

Hit# Of 5 ntative ID . MW MolForm CAS# Qual

l Phenanthrene-d10 188 C14D10 001517-22-2 43 2 Anthracene-d10- 188 C14D10 001719-06-8 39 3 4H-Pyrido[l , 2-a] pyrimidin-4-one, 3- 188 C11H12N20 057773-19-0 38 4 Benzene / l-bromo-4-methoxy- 186 C.7H7BrO 000104-92-7 33 Abundance Scan 2269 (25.873 min): 4024.D (-) m/ z 188.10 100.00% 188

! i 5000

' . ............... — 66 78 92 158 . —L 25.60 25.80 26.00 26.20

miz-> 4 LT 4 I-.............. O' ’ 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 i ■ ■ ■ • i T m/ Z 184.05 15.24% Abundance #19958: Phenanthrene-d10 188

5000 25.60 25.80 26.00 26.20 80 160 m/ z 18 9.10 13.44% 94 11111' I'11111 ‘11111'11' 66 I - T’’t 11111. ।.... ।. TTTI 11111 all 111111 m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19957: Anthracene-d10-

I 188 _ / i ■ 1 T 25.60 25.80 26.00 26.20 5000 m/z 91.90 12.76%

rk ............. 66 80 ........... ,l94 TTTTT ri 111111111111111111 ■■ 1111 160 i ■ ■«• i • ■ ■ ■ i > ■ ■ • i ■ ■ ■ • i ■ ■ > > TTTTITT 111111 rrf m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19873: 4H-Pyrido[1,2-a]pyrimidin-4-one, 3-ethyl-6-methyl- - 145 188 25.60 25.80 26.00 26.20 173 11:35% 5000 92

65 159 | । . . .119 . 132 +— — 111111 ■ ■ I > • • • t ■ •1111 i PTPIT ■■■■-!■ I . . । । .। ।।।i>। . I T’T T 'm/z—> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 25.60 25.80 26.00 26.20

4024.D GCMS0208.M Wed Mar 13 11:39:13 2002 Page 4

NYC-WTC_000038312

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NYC-WTC_000038312Source: NYC Law Department, mirrored locally

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