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GCMS sample AE07107 results, April 2002

Machine-extracted title · confidence 95%

Laboratory report of GCMS analysis for sample AE07107 including surrogate recovery data from April 29, 2002.

NYC-WTC_000043472–000043481

Folder label: “GCMS X 4/23/02 A 4/24/02

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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C : \HPCHEM\ 1 \DATA\APR24027107.D Vial : 13 Acq On : 25 Apr 2002 3:27 am Operator: Sample : gc/ms scan 4/23 Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Phenanthrene-dlO Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

25.72 0.21 ug/1 44165 Phenanthrene-dl0 25.59

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Phenanthrene -dl 0 Z 7 188 C14D10 001517-22-2 72 2 Naphthalene, 1,7-dimethoxy- 188 C12H1202 005309-18-2 42 3 Anthracene-dl0 - 188 C14D10 001719-06-8 42 4 Antipyrine____ 188 C11H12N2O 000060-80-0 40 Abundance 7 Scan 2252 (25.723 min): 7107.D (-) m/z 188.10 100.00% 188

5000 t । । । । 4 S । r । । । । i — । । । । |"

80 94 160 25.40 25.60 25.80 26.00 44 64 | |11" i ■ ■■ ■ i ■1 " r । [ 1111111111 TWTTTTTTTTI । । । । i l'l । । । । m/z 189.10 13.30% rn/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19958: Phenanthrene-d10 188

5000 ------- 25.40 25.60 25.80 26.00 m/ Z 79.95 12.59% 94 80 160 66 1 I I I । । I I I I | I I I 1 | I'।'। L I I ! I — i 11 ■ • r '1 1 I ■'1 11 m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19913: Naphthalene, 1,7-dimethoxy- 173 188 i । [ ,1 । । । — [ । । । । j—i i । । r

25.40 25.60 25.80 26.00 5000 m/z 184.10 9.04% 102 115 145 51 63 75 158 94 130 | m/z-> 1" I" 1 TT TIT 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 ■ i'11' i' Ti Illi [ I I I I I I I > I I I

Abundance #19957: Anthracene-d10- 1 1 i ' 1 1 1 i1 ' 1 ITIrU 1 I ' 1 1 1 I 188 25.40 25.60 25.80 26.00 m/ z 93.95 8.36% 5000

p। 80I 94 J 160 ■■i■■'■i ■ ■■ ■ i - • I ■ i ■' ■ 11 ।11''11'1111111111'1111 " 11 11 " 11 r 1‘I Til ' i 1 1 1 ■ i m/z—> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 25.40 25.60 25.80 26.00

7107.D GCMS0412.M Thu Apr 25 11:16:48 2002 Page 2

NYC-WTC_000043480

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NYC-WTC_000043480Source: NYC Law Department, mirrored locally

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