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GCMS analysis results for sample AE05901, March 29 2002

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Laboratory report detailing GCMS analysis of environmental sample AE05901 conducted on March 29, 2002.

NYC-WTC_000059799–000059808

Folder label: “GCMS X 3/13/02 A 3/27/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\MAR2 202\5901.D Vial: 30 Acq On : 22 Mar 2002 7:07 pm Operator: Sample : gc/ms scan 3/13 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ******★*★★★***★******★★**★*★************★******★*★********★*★★***★★★* Peak Number 1 Phenanthrene-dlO Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

25.79 0.20 ug/1 29671 Phenanthrene-dl0 25.65

Hit# of 5 Tentative / ID MW MolForm CAS# Qual 7----------- .--- 1 Phenanthrehe-dlO 188 C14D10 001517-22-2 87 2 Anthraceny-dlO- 188 C14D10 001719-06-8 86 3 Naphthal^e, 1,7-dimethoxy- 188 C12H12O2 005309-18-2 50 4 Pentacy^o[8.4.0.0(3,7) .0(4,14) .0(6 188 C14H20 000000-00-0 42 Abundance ( Scan 2260 (25.790’min)T590i ............. m/z 18 "‘id. "‘idd‘.’oo% 1$8

5000 I \ •p-r* 43 66 80 158 25.40 25 60 25.80 26.00 26.20 ... ................... . -X-T IT m/z 18 9.05 14.03%' m/z->.... ...... 40 50.... 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19958: Phenanthrene-dlO 1(!8

5000 25.40 25.60 25.80 26.00 26.20 80 04 160 m/z 80.05 13.38% 66 I V I,, i, I, ,,, I,,,, I;!. p-m-j- __ 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #'9957: A.ritfnacenc-d’0- 188 -f-r-e 25.40 25.60 25.80 26.00 26.20 5000 m/z 184.05 12.88% 1

cc 66 80 94 160

m/z-J.,____ 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 ‘Abundance #19913; Naphthalene, 1,7-dimethoxy- / 173 1^8 25.40 25.60 25.80 26.00 26.20 m/z 92.00 12.08% 5000 102 115 145 94 130

40 50 60 70 i80 90 100 110 120 130 140 150 160 170 180 190 25.40 2^0 25^0 2^6W 26JO

5901.D GCMS0308.M Mon Mar 25 14:32:23 2002 Page 1

NYC-WTC_000059806

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NYC-WTC_000059806Source: NYC Law Department, mirrored locally

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