GCMS analysis results for sample AE05901, March 29 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\MAR2202\5901.D Vial: 30 Acq On : 22 Mar 2002 7:07 pm Operator: Sample : gc/ms scan 3/13 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Isopropyl Palmitate Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

28.15 1.47 ug/1 215654 Phenanthrene-dlO 25.65

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Isopropyl Palmitate 298 C19H38O2 000142-91-6 35 2 HexadecanoA: acid 256 C16H32O2 000057-10-3 35 3 Octadecano^ic acid 284 C18H3 6O2 000057-11-4 20 i me t by 1 s1 y 1) 3 - me t hoxy t y r ami 311 C15H29NO2Si2 000000-00-0 14 Abundance Scan 2517 (28J49 min); "5^ (-) m/ Z 4|3 102 60 5000 256 129 239 I l-T ■11^ I ^43 157 171 185 igg 213 ^27’ l| |l. 293 27.80 28.00 28.20 28.40 I..32... 1 m/z 102*. 05 66.83% m/z->_____ .40__ 60. 80.. ipp. 120 140 160 180 200 220 240 260 280 300 Abundance #4'2488: Isopropyl Palmitate 162

5000 60 73 129 _22,8p_ 28.p0_2_8Jp_28^ __ 85 m/z’ ”6o'. 05 " '61.”57% 157 257 'm/z->_____ 40__ 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #15186. Scxadecanoic acid 43 60 73 I 27.80 28.00 28.20 28.40_____ 5000 m/z 41.05 53’. 79% 97 •129 ! 1 157 171 185 213 256

'm/z-> Abundance .. 40. 60

f 60 ? 80 100 120 140 160 ,180 2OO #72363: Octadecanoic acid 220 240 260 280 300 .....n... 27.80 28.00 28.20 28.40 m/z 57.0,0 43.05% 5000 129 97 241 284 4 I T, •171 ' '' ' I ' 222 I ' I ' ' ' ' I ' \ 40 60 80 100 120 140 160 180 200 220 240 260 280 300 27-.8P_28.pO, 28.20 28/40

5901.D GCMS0308.M Mon Mar 25 14:32:27 2002 Page 2

NYC-WTC_000059807