GCMS blank analysis results for sample AE01156, March 25 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\MAR2102\LBA.D Vial: 16 Acq On : 22 Mar 2002 2:05 am Operator: Sample : gc/ms scan 3/13 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Hexadecanoic acid Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

28.15 0.34 ug/1 91834 Phenanthrene-dl0 25.66

Hit# of 5 Ten^tive ID MW MolForm CAS# Qual

1 Hexadecanoic aoid 256 C16H32O2 000057-10-3 38 2 Isopropyl Palmitate 298 C19H38O2 • 000142-91-6 35 3 3-Ethylheptanbic acid 158 C9H18O2 014272-47-0 25 4 . alpha.-D-GLticopyranoside, methyl 3 176 C7H12O5 013407-60-8 23 Abundance..... ....... '..... .... Scair25T7(2Sl5T^^ m/z. '437X5.. 43 60 102 5000 73 256

m/z-> Abundance 20 J 40

413 Uu 60

60 7fl 80 100 nil 120 129

140 157 171 185 199 213 160 #71607; Hexadecanoic acid 180 200 220 239 I__ L 240 .

260 ............ I.l.......... 27.80 28.00 28.20 28.40 m/z 60.05 65.62% I*

.................... j \................. 5000 256 129 27.80 28.00 28.20 28.40 97 213 m/z 102.05 60.82% ! m/z-> ■ 4™-r 20 40 _60___80__ 100 11 120 ! 140 157 171 i I r-r-|-r-r-r-j 160 180 200 I 227 220 240 260 Abundance /f42488 Isocrcpyl PaSmitate 102

27.80 28.00 28.20 28.40 5000 60 m/z 41.05 55.29% 73 129 85 157 257 m/z->__ 20 Abundance 40 60 £7 80 100 120 140 160___ 180 #11989: 3-Ethylheptanoic acid 200 220 240 260 l\ 27.80 28.00 28.20 28.40 m/z 57.00 52.27% 5000 ■

27 98

'm/z-> 20 40 1 I !. , ,... I... ............. 60 80 129

100 120 140 160 180 200 220 240 260 27.80 28.00 28.20 28.40

LBA.D GCMS0308.M Mon Mar 25 14:30:27 2002 Page 2

NYC-WTC_000059677