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GCMS analysis results for sample AE05900, March 29 2002

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Laboratory report detailing GCMS analysis of environmental sample AE05900 conducted on March 29, 2002.

NYC-WTC_000059788–000059798

Folder label: “GCMS X 3/13/02 A 3/27/02

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Scanned page image, NYC-WTC_000059796
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\MAR2202\5900.D Vial: 29 Acq On 22 Mar 2002 6:07 pm • Operator: Sample gc/ms scan 3/13 Inst : GC/MS 209 Mise Multiplr: 1.00 MS integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title • : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ★★*★****★*★*★*★**★★★*****★★****★**★*********★★★★★*★★*★*****★*★★★***** Peak Number 2 Isopropyl Palmitate Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

28.15 9.95 ug/1 1717500 Phenanthrene-dl0 25.66

Hit# of 5 ntative ID MW MolForm CAS# Qual

1 Isopropyl Palmitate 298 C19H38O2 000142-91-6 43 2 Hexadecangle acid 256 C16H32O2 000057-10-3 35 3 Octadecanoic acid 284 C18H36O2 000057-11-4 20 4 Urea, (2-chiazolin-2-yl)- 145 C4H7N3OS 015823-99-1 16 Abundance......... .... .............................Sratr2^1(28?i497^^ m/ z 43 . OS 4b ft 60 102

5000 73 256 129 239 ''r T~' I 115 J 143 157 171 185 199 213 27.80 28.00 28.20 28.40 298 m/z 102.OS 65.89% m/z->40 60 JBO. 100 120 140 160 180 200 220 240 260 280 300 Abundance ................ #42488: Isopropyl Palmitate 102

5000 60 I 73 129 27,80 28,00 28,20 28.40 ?5 ! m/ z 60.05 62.41% i Ill Ji lU I .m/z->40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance ^*35"'86: Hiexadewncic acid « 60 73 ! ~T 27^ 28,00 2^0 28.40 5000 m/ Z 41.05 54.55% 97 129 j 157 171 185 213 256 i I m/z->40. 60. 80 'Abundance 4)3 100 120. 140 160 180 200 220 #72363: Octadecanoic acid 240 260 280 300 1 TT-T

60 T . 27.80 28.00 28.20 28.40 m/z 57.0,0 4676^ 5000 85 97 129 Il 111 185 241 284 171 222 I ............ .. , m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 27.80 28.00 28.20 28.40

5900.D GCMS0308.M Mon Mar 25 14:31:29 2002 Page 2

NYC-WTC_000059796

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NYC-WTC_000059796Source: NYC Law Department, mirrored locally

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