GCMS analysis results for sample AD29783, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC1401\29783.D Vial: 6 Acq On 15 Dec 2001 7:25 am Operator: 209 GALOS Sample : gems scan 12/10 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 3 Butane, 2,3-dichloro-2-methyl- Concentration Rank 8

R.T. EstConc Area Relative to ISTD R.T.

7.21 0.73 ug/1 212417 1,4-Dichlorobenzene-d4 11.67

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Butane, 2,3-dichloro-2-methyl- 140 C5H10C12 000507-45-9 56 2 Propane, 2-bromo-1-chloro- 156 C3H6BrCl 003017-95-6 28 3 1-Propene, 1-chloro- 76 C3H5C1 000590-21-6 9 4 Propane, 2-chloro-2-nitro- 123 C3H6C1NO2 00059.4-71-8 9 Abundance Scan 236 (7.208 min): 29783.D (-) m/z 76.95 100.00% I 77 41 5000

- -------- I 53 63 80 i9 105 I. 125 207 6.80 m/ z 7.00 41.05 7.20 7.40 7.60 61.24% m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 'Abundance #7245: Butane, 2,3-dichloro-2-methyl- 77

5000 6.80 7.00 7.20 7.40 7.60 27 m/z 75.90 4 4.90% 53 63 89 105 _......I 125 V r " 'i " ■ । ■ r i r "' i i1"' i"' m/z-> 20 30 40 50 60 7 0 80 90 100 110 120 130 140 150 160 170 180 190 200 210 Abundance #67227: Propane, 2-bromo-1-chloro- 77 - 1 Dmm— T , , TT 6.80 7.00 7.20 7.40 7.60 5000 41 m/z 78.95 33.23%

27 107 158 i 61 IT TURmgTTTTpugauT ‘ i" " r "111'" i m/z-> :20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 — Abundance> #367: 1-Propene, 1-chloro- T Tf T- । i । > < 41 6.80 7.00 7.20 7.40 7.60 m/z 69.00 29.75% 76 5000-

m/z-> —H TTTIm 1 — ———————— 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 6.80 7.00 7.20 7.40 7.60

29783.D GCMS1126.M Fri Dec 28 13:15:09 2001 Page 3

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