GCMS analysis results for sample AD29783, Jan 2002

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Laboratory report of GCMS analysis for sample AD29783 conducted on January 7, 2002.

NYC-WTC_000037052–000037070

Folder label: “GCMS X 12/10/01 A 12/15/01”

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NYC 9/11 Public Portal Document

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Data File : C:\HPCHEM\1\DATA\DEC1401\29783 .D Vial: 6 Acq On 15 Dec 2001 7:25 am Operator: 209 GALOS Sample : gems scan 12/10 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Amylene Hydrate Concentration Rank 9

R.T. EstConc Area Relative to ISTD R.T.

6.76 0.67 ug/1 194679 1,4-Dichlorobenzene-d4 11.67 !

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Amylene Hy drate 88 C5H120 000075-85-4 39 2 3-Pentanol 88 C5H120 000584-02-1 38 3 4-O-Ac/tyl-2,5-di-O-methyl-3,6-dide 215 C10H17NO4 000000-00-0 38 4 Acetamide 59 C2H5NO 000060-35-5 9 Abundance Scan 187 (6.758 min): 29783.D (-) m/ z 59.0,5 100.00% 59

5000 43

107. 6.40 6.60 6.80 7.00 7.20 11" 11..........1 1450. +7787 ,. 36 I'' ■ ■ I'''’i■•■' i11'' i • ■ ■•i■■ ■ ■ i ■ ■ ■' i • ■'•i1■ ■ ■ i ■ ■ • ■ i' ■''i TT m/ z 43.0.0 44.23% mlz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #62938: Amylene Hydrate 59

73 5000 31 43 6.40 6.60 6.80 7.00 7.20 m/ z 41.00 16.78% .1 1 , i 1 ■ ' ■ i ' ■ ■ ' i ■ miz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #62942: 3-Pentanol .. . .. 59 1 31 6.40 6.60 6.80 7.00 7.20 5000 m/z 107.00 16.53% 1 41 _ _____________ 87____________________________________________ 1' i ■ ■ ■' i'' ■ ■ i' " ■ i' ■ ■' i ■' " r " ■ i " ■ • i' ■'' i " " r ■ " i " ' • i ■ " ' i " '' r " ' r ■ " i " " i' m/z-> 20 30 40 50 60_ 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #26486:4-O-Acetyl-2,5-di-O-methyl-3,6-dideoxy-d-gluconitri ........— — —A 59 6.40 6.60 6.80 7.00 7.20 m/z 69.00 5.78% 5000 43

■ i'' ■' r ''' i TTT ' i' 85 97 113 156 173 ■ ■ i ■ TIMnT TT1T 1V miz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 6.40 6.60 6.80 7.00 7.20

29783.D GCMS1126.M Fri Dec 28 13:15:02 2001 Page 2

NYC-WTC_000037060

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NYC-WTC_000037060Source: NYC Law Department, mirrored locally

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NYC-WTC_000036542

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