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GC/MS analysis results for sample AD23320, Oct 2001

Machine-extracted title · confidence 90%

Laboratory report documenting GC/MS analysis of sample AD23320 conducted on October 15, 2001.

NYC-WTC_000088207–000088236

Folder label: “GC/MS Scan 9/25/01

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Scanned page image, NYC-WTC_000088218
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1201\23320.D Vial: 13 Acq On : 12 Oct 2001 1:51 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 1,4-Dichlorobenzene-d4 Concentration Rank 18

R.T. EstConc Area Relative to ISTD R.T. 11.62 0.50 ug/1 46279 1,4-Dichlorobenzene-d4 11.77 Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 1,4-Dich robenzene-d4 150 C6C12D4 003855-82-1 42 2 Benzene ,2,3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 25 3 Acenap: hylene 152 C12H8 000208-96-8 9 4 Biphe: lene 152 C12H8 000259-79-0 9 Abundance Scan 717 (11.619 min); 23320.D (-) m/z 149.90 100.00% 1!i0

553 115

52 78 41 I 63 11.20 11.40 11.60 11.80 12.00 ' ' I ' ' 'I . I I H . I ..........5 II m/z 151.90 63.58% Tife-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9593:1,4-Dichlorobenzene-d4 1!10

253 115 78 11.20 11.40 11.60 11.80 12.00 52 m/z 115.00 37737% 35 nte-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 ^bundance #9592; Benzene-1,2,3,4-d4-, 5,6-dichloro- liiO I ' ' ' ' I ' ' 115 11.20 11.40 11.60 11.80 12.00 5000 52 78 m/z 77.95 20.28%

87

■n/z-> 30 35 I ‘ I ' ' ' ' I 40 50 ' ' ' I ' ' ' ' I ‘ ' 60 70 80 I ‘ I 90 100 A 110 120 130 140 ■i. 150 160 Abundance #67015: Acenaphthylene 1:2 11.20 11.40 11.60 11.80 12.00 “mTz 52.00 14.79%

253 76 ,il 87 98 T-ryT-T-T-T-yT-T-T-T-yT-T-rT-ytVT-r-p4H-ryT-T-TT-yrT-rTq-T-rT’TyTT-TT-yT-T-in-^^ 126 II ■n/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 11.20 11.40 11.60 11.80 12.00

23320.D NP091101.M Mon Oct 15 09:53:41 2001 Page 5

NYC-WTC_000088218

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NYC-WTC_000088218Source: NYC Law Department, mirrored locally

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