GCMS unknown compound analysis, sample AE05515, April 2002

NYC 9/11 Public Portal Document

-c Library Search Compound Report

Data File C:\HPCHEM\1\DATA\APR0102\5515.D Vial: 6 Acq On l.Apr 2002 4:11 pm Operator: Sample gc/ms scan 3/11 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 6 Butane, 1,3-dichloro-3-methyl-. Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

9.70 20.24 ug/1 3418210 1,4-Dichlorobenzene-d4 12.25

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Butane, 1,3-di^loro-3-methyl- 140 C5H10C12 0.00624-96-4 36 2 1-Pentene, 3-^omo-4-methyl- 162 C6HllBr 000815-47-4 27 3 Butane, 2,3-^chloro-2-methyl- 140 C5H10C12 000507-45-9 22 4 2-Butene, l/bromo-3-methyl - 148 C5H9Br _______ 000870-63-3 16 Abundance ” Scan 507 (9;697 mih): 5515.0 (-) m/z " ■ 41.05* “10^0% 4|1 69 105

I 5000

h/z-> __ 20 '' I'' 53 77

171 186 121 . i-|133141 ' I'''' I'''' I 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 149 II . . . . I I . . . I J .. L 9.40 m/z 104.95 9.60 9.80 10.00 93.92% Abundance #7246: Butane, 1,3-dichloro-3-methyl- 69 41 77 5000 27 9.40 9.60 9.80 10.00 53 105 m/ z 87.18% rUrrnT-rr Ju I'''' I''' * I I' ‘' I

Jk n^-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #12782: 1-Pentene. 3-t:romo-4-methyl-

i 6,9 9.40 9.60 9.80 10.00 5000 m/ z 51.28% !

m/z-> T +t 53 i li, 106 ■ 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 148 I'''' I

ftbundance #7245: Butane, 2,3-dichloro-2-methyl- 7|7 9.40 9.60 9.80 10.00 m/ Z 39.05 32.81%

L 5O0O 69 27 53 105 I 35 I 1 89 I 125 fn/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 9.40 9.60 ' 9.80 10.00

5515.D GCMS0403.M Thu Apr 04 13:53:12 2002 Page 6

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