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GCMS analysis results for sample AE05701, April 2002

Machine-extracted title · confidence 90%

Laboratory report documenting GCMS analysis of sample AE05701 conducted on April 11, 2002, including surrogate recovery data.

NYC-WTC_000059508–000059516

Folder label: “GCMS X 3/12/02 A 4/2/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\APR0102\5702.D Vial: 20 Acq On 2 Apr 2002 7:05 am Operator: Sample gc/ms scan 3/12 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library .: C:\DATABASE\NBS75K.L * * * * *,* *************************************************************** Peak Number 1 Silane, tetramethyl- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

8.13 1.83 ug/1 289357 1,4-Dichlorobenzene-d4 12.25

Hit# of 5 Tentative ID MW MolForm CAS# Qual -----------------/_ 1 Silane/ tetramethyl- 88 C4H12Si 000075-76-3 28 2 N-Ethylformamide 73 C3H7NO 000627-45-2 9 3 1,3-Dioxolane, 2-pentadecyl- 284 C18H36O2 004360-57-0 9 4 1,3-yioxolane, 2-methyl- 88 C4H8O2 ________000497-26-7 7 Abundance Scan336)(8J^^ m/’z ' '7 3 .To"'" ' 100"".""00"% 7t3

5000 43 , ............... 57 87 103 7.80 8.00 8.20 8.40 1 ilil -ryv- m/z 43.0,5 30.67% 'm/z->20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #845: Silane, tetramethyl- 70

5000 -_2;:80_8,00__a20___8^^ m/z 45.05 10.61% 88 m/z->20 40 60 80__ 100 120 140 160 180 200 220 240 260 280 Abundance '4292; N-Ethyllnrrnarnioe 30 73 7.80 8.00 8.20 8.40 5000 m/z 41.0.5 10.09% 44 58

'm/z-> 20 40__ 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #40191; 1,3-Dioxoiane,2-pentadecyl- 70 7.80 8.00 8.20 8.40 m/ Z 71.00 6.51% 5000

43 57 86 99 256 283 20 40 60 80 100 120 140 160 180 200 220 240 260 280 7.80 8.00 8.20 8.40

5702.D GCMS0403.M Eri Apr 05 10:35:00 2002 Page 1

NYC-WTC_000059515

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NYC-WTC_000059515Source: NYC Law Department, mirrored locally

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