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GCMS analysis results for sample AE05702, April 2002

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Laboratory report documenting GCMS analysis of sample AE05702 conducted on April 11, 2002, including surrogate recovery data.

NYC-WTC_000059517–000059525

Folder label: “GCMS X 3/12/02 A 4/2/02

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Scanned page image, NYC-WTC_000059524
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\APR0102\5703.D Vial: 21 Acq On 2 Apr 2002 8:04 am Operator: Sample gc/ms scan 3/12 fb Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Silane, tetramethyl- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

8.13 1.84 ug/1 260140 1,4-Dichlorobenzene-d4 12.25

Hit# of 5 Tentative ID MW MolForm CAS# Qua! 1 Silane, ,-^tramethyl- 88 C4H12Si 000075-76-3 47 2 N-Ethyl'formamide 73 C3H7NO 000627-45-2 9 . 3 Pentahe, 3-methoxy- 102 C6H14O 036839-67-5 9 4 l,3-p(ioxolane, 2-pentadecyl- 284 C18H36O2 004360-57-0 9 Abundance 7-...... . ....... .... ........... Scan 336 (8J27 min):‘5703.b (-)’ m/z 73.00 : 7|3

! i 5000 43 I ' ' ' ' I 7.80 8.00 8.20 8.40 I 49 55 6L I I . 103 ' 'I > ' '' ‘ ‘ I m/z 43.05 27.84% m/z->10 20 30 40 50 60 70 80 90 100 110 Abundance #62932: Silane, teframethyl- 7)3

J 5000 7.80 8.00 8.20 8.40 45 m/z 41.05 10.86% 15 .1 53, 59 I 88 m/z--> 10 20 30 40 50 60 70 80 90 100 110 Abundance #292; N-EtHylformariiide i 30 I 73 .. / i 7.80 8.00 8.20 8.40____ 5000 m/ z 45.05 10.04%

15 44 58 (f m/z-> 10 20 30 40 __ 50____60____ 70___ 80 90 100 110 Abundance #1793: Pentane, 3-methoxy- ...................... ................................ I 713 7.80 8.00 8.20 8.40 ___ m/z 7.20% I 5000 i 45 i i V 33 3,9, m/z-> 10 20 30 40 50 60 70 80 90 100 110 7.80 8.00 8.20 8.40

5703.D GCMS0403.M Fri Apr 05 10:35:35 2002 Page 1

NYC-WTC_000059524

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NYC-WTC_000059524Source: NYC Law Department, mirrored locally

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