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GCMS analysis results for sample AE05851, April 17 2002

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Laboratory report documenting GCMS analysis of sample AE05851 conducted on April 17, 2002, including surrogate recovery data.

NYC-WTC_000059650–000059659

Folder label: “GCMS X 3/12/02 A 4/4/02

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\HPCHEM\l\DATA\APR04 02\5851.D Vial: 25 Acq On 4 Apr 2002 9:45 pm Operator: Sample gc/ms scan 3/12 Inst : GC/MS 209 Mise Multiplr: 2.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0408.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Silane, tetramethyl- Concentration Rank 1

R.T. ' EstConc Area Relative to ISTD R.T.

8.13 7.19 ug/1 347868 1,4-Dichlorobenzene-d4 12.25 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Silane, tetramethyl- 88 C4H12Si 000075-76-3 37 2 N-Ethylformamide 73 C3H7NO 000627-45-2 9 3 Pentane, 3-methoxy­ 102 C6H14O 036839-67-5 9 4 1,3- ioxolane, 2-(3-bromo-5,5,5-tri 352 CIOH16BrC13O2 000000-00-0 9 Abundance 1 Scan 336 (8.127 min): 5851 .D (-) m/z 73.00 100.00%! 7b

5000 43

87 7.80 8.00 8.20 8 40 I 50 ,57 67, 1 103 Un-.... ' ' I ' ' ' 'I ' ' ' 'I' ' ' ' I ' ' I ' m/z 43.05 27.37% nZz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #845: Silane, tetramethyl- 7b

5000 7.80 -U 8.00 8.40

45 m/z 41.05 10.68% j 15 31 . ... I , , , , , .... TiZz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #292: N-Ethytformamide 3b 73 7.80 8.00 8.20 8.40 5000 m/z 45705 10.08% 44 58

I ' ’ ' ' I ' - n444^ ■n/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #1793: Pentane, 3-methoxy- 7b 7.80 8 00 8.20 8.40 m/z 71700 6758% 5000 45

7,33 . ?l. 55 ' I ' ''' '' I ' ' ' ' I' I ■nA'-> 10 20 30 40 50 60 70 80 90 icX) 110 ' 7.80' 8.00 8.20 8.40

5851.D GCMS0408.M Tue Apr 16 08:18:08 2002 Page 1

NYC-WTC_000059657

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NYC-WTC_000059657Source: NYC Law Department, mirrored locally

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