NYC-WTC_000046249
Calibration table data for GCMS analysis of volatile organic compounds dated May 3-6, 2002.
1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗Document / 25 pages
GCMS analysis results for sample AE11602, June 2002
Machine-extracted title · confidence 90%TCLP calibration table document dated May 24, 2002, listing deuterated standards and response factors for GCMS analysis.
NYC-WTC_000013943–000013967Folder label: “GCMS X 5/24/02 A 5/28/02”
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OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File : C:\HPCHEM\1\DATA\MAY2102\11602.D vial: 31 Acq On : 22 May 2002 8:06 pm Operator: Sample : EXTRACTS/20 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P =
Quant Method : C:\HPCHEM\1\METHODS\GCMS0520.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C: \DATABASE\NBS75K. L ********************************************************************* Peak Number 16 1-Hexanol, 4-methyl- Concentration Rank 2
R.T. EstConc Area Relative to ISTD R.T. 13.51 8.55 ug/1 548916 1,4-Dichlorobenzene-d4 12.15
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 1-Hexanol / 4-methyl- 116 C7H160 000818-49-5 37 2 Cyanic aoad, sec-butyl ester 99 C5H9NO 001873-13-8 37 3 Octane, -propoxy- 172 C11H240 029379-41-7 36 4 Methyla line, N- (1-ethylpentylidene) 127 C8H17N 018641-73-1 33 Abundance * Scan 924 (13.511 min): 11602.D (-) m/z 43.05 100.00%| 43 70
5000
............... I ■ ।" " । • ■ ■ ■ i ■ +op 53 14 61
———191 TI—83, 115 puuauumT Ml ■ ■ 1 1 1 ‘ 1 i 13.20 13.40 13.60 13.80 m/z 70.05 70.61 miz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 Abundance #3348:1-Hexanol, 4-methyl- 41 70
5000 29 56 AM ~r' • • ■ i 1 ■ 1 ■ i 13.20 13.40 13.60 13.80 m/z 69.05 47.15 ... 83 98 — ’118 . 1... I (( i ... tt , miz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 Abundance #1408: Cyanic acid, sec-butyl ester 70 1 • ■ 1 ■ i ■ ■ • • i 41 13.20 13.40 13.60 13.80 5000 m/z 41.00 43.64 56 27 84 — # , | 99, mfa-> Abundance pp 1133 20 30 40 50 60 70
43 80 90 100 110 120 130 140 150 160 170 #15849: Octane, 1-propoxy- AW - 13.20 13.40 13.60 13.80 m/z 61.05 34.53 5000 57 71
miz—> 27 TIWmp ’ 1’4 97 "l“ “I'"''I1 112 143 83
17 172 11" “ i ■■■ ■ ■ i ■ ‘ ' i ■ “ ■ i' ■ “ i 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 AMA).... . 1 13.20 13.40 13.60 13.80'11
11602.D GCMS0520.M Fri May 24 08:33:18 2002 Page 16 NYC-WTC_000013963
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NYC-WTC_000013963Source: NYC Law Department, mirrored locally
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1 shared topics · similarity 0.988
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1 shared topics · similarity 0.988
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000024997
Laboratory report documenting GCMS analysis of sample AE11309 conducted on May 28, 2002, including surrogate recovery data.
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