GCMS analysis results for sample AE11602, June 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\l\DATA\MAY2102\11602.D Vial: 31 Acq On : 22 May 2002 8:06 pm Operator: Sample : EXTRACT5/20 Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P g*.* Quant Method : C:.\HPCHEM\1\METHODS\GCMS0520 .M (RTE Integrator) me Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 17 Acetic acid, heptyl ester Concentration Rank 8 R.T. EstConc Area Relative to ISTD R.T. 14.09 2.33 ug/1 183474 Naphthalene-d8 15.77 Hit# of 5 ntative ID MW MolForm CAS# Qual 1 Acetic acid, heptyl ester 158 C9H1802 000112-06-1 78 2 Acetic acid, octyl ester 172 C10H20O2 000112-14-1 78 3 Acetic acid, hexyl ester 144 C8H1602 000142-92-7 42 4 Acetic acid, decyl ester 200 C12H2402 000112-17-4 42 Abundance Scan 987 (14.089 min): 11602.D(-) m/z 43.05 100.00% 43

5000 — 56 70 61 13.80 14.00 14.20 14.40 38, tr +1+1 83 88 116 1 ■ i ‘ 1 1 ‘ i 1 1 ■' ‘ i' ■ ' ■ ‘ i 1 ‘ 1 1 i ‘ 1 m/z 56.10 41.36% niz-> 20 30 40 50 60 70 80 90 100 110 120 Abundance #11981: Acetic acid, heptyl ester 43

5000 56 13.80 14.00 14.20 14.40 70 61 m/z 70.05 33.49% 27 I , i i ■ ' i ■ ‘ 89 *6 116 ■ i ■ ■ ■ 1 i • • ■ • i ■ ■ ■ • i ■ ■ niz-> 20 30 40 1 50 ' 60 7080 90 100 110 120 Abundance #68338: Acetic acid, octyl ester 43

13.80 14.00 14.20 14.40 5000 m/z 55.10 26.80% 56 . 61 70

N 84 112

■ i • 1 ■ ■ I ' 1 1 1 1 ‘ ‘ I ‘ ‘ I, i • ■ ), 1 ' ' l ' ' iz-> 20 30 40 50 60 70 80 90 100 110 120 Abundance #66310: Acetic acid, hexyl ester ■ A Di 43 13.80 14.00 14.20 14.40 m/z 61.05 25.95% 5000 56 61 27 69 84 | < t * * ' > i • ■ • 'i1 ' ‘ I ' ‘ 1Ir _1 ' ' i ‘ ■ 1 ' i ‘ 1 • ■ i ' • • ■ i ■ ‘ ■ i ' ■ • ■ i ■ ■ mfz-> 20 30 40 50 60 70 80 90 100 110 120 13.80 14.00 14.20 14.40

11602.D GCMS0520.M Fri May 24 08:33:19 2002 Page 17

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