GCMS analysis results for sample AE11602, June 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\MAY2102\11602.D Vial: 31 Acq On : 22 May 2002 8:06 pm Operator: Sample : EXTRACTS/20 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0520.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C: \DATABASE\NBS75K. L . ********************************************************************* Peak Number 18 1-Decanol Concentration Rank 12 R.T. EstConc Area Relative to- ISTD R.T. 14.27 1.11 ug/1 87397 Naphthalene-d8 15.77 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 1-Decanol 158 C10H22O 000112-30-1 50 2 Isooctanol 130 C8H180 026952-21-6 43 3 1-Octene 112 C8H16 000111-66-0 42 4 1-Ocene, 3,7-dimethyl- 140 C10H20 004984-01-4 33 Abundance Scan 1007 (14.272 min): 11602.D (-) m/z 43.05 100.00% 43

5000 57 ............... ................................ - 70 83 i . 97 14.00 14.20 14,40 14.60 1, 11 Pi ■ 51p’ii 11 H— .... ,88, a 112 •r r | / P) > m/z 57.10 43.00% mfz-> 20 30 40 50 60 70 80 90 100 110 120 Abundance #67467:1-Decanol 43

—A 55 70 5000 83 14.00 14.20 14.40 14.60 31 m/z 55.10 41.53%

niz—> 20 30 40 • • i • • 50 ' I ' ' 70 60 80 ... "....‘12.... 90 100 110 120 Abundance #65281: Isooctanol 43 55 69 enn 184 .B3T 14.00 14.20 14.40 14.60 5000 84 m/z 56.10 40.71% 27 __ 97 I ■ i ' ■ ■ ■ l rl ' ' I ■ ■ i 1 ■ ‘I* ■ ■ i ' ‘ • i 1 ■ ■ ■ i ■ ■ • 1 i ‘ ■ miz-> 20 30 40 50 60 70 80 90 100 110 120 Abundance #2657:1-Octene 43 14.00 14.20 14.40 14.60 55 m/z70.15 33.70% 70 5000 27

/z-> 111+*I‘‘‘‘I 20 30 40 ■ ' i ‘ ‘ 50 H— 60 — 70 83 I........ 97.......... 112.......... *• । > i * - | । i ■ , । । । । i । i 80 90 100 110 । 1 । 120 A 14.00 14.20 14.40 14.60

11602.D GCMS0520.M Fri May 24 08:33:20 2002 Page 18 NYC-WTC_000013965