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GC/MS analysis results for sample AD23837, Nov 1 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GC/MS analysis of sample AD23837 conducted on November 1, 2001, identifying unknown compounds.

NYC-WTC_000089333–000089345

Folder label: “GC/MS Scan 10/1/01

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Scanned page image, NYC-WTC_000089342
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\OCT3001\23837.D Vial: 11 Acq On : 31 Oct 2001 12:17 am Operator: 2 09 GT^LOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 7.70 0.72 ug/1 191586 1,4-Dichlorobenzene-d4 11.71 Hit# of 5 T^tative ID MW MolForm CAS# Qual 1 2-Pentanol^ 4-hydroxy-4-methyl- 116 C6H12O2 000123-42-2 39 2 2-Hexano^ 2-methyl- 116 C7H16O 000625-23-0 17. 3 Acetic cid, cyano-, 1,1-dimethylet 141 C7H11NO2 001116-98-9 12 4 Aceton 58 C3H6O 000067.-64-1 9 Abundance Scan 289 (7.700 min): 23837.D (-) m/z 42795 100.00% . 43

59 5000 101 ............................. I 83 7.40 7.60 7:80 8.00 35 I 71 m/z 59.05 53.37% nZz-> 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #3245: 2-Pentanone, 4-hydroxy-4-methyl- 43

5000 59 7.40 7.60 7.80 8.00 m/z 101.05 23747% 31 I .... 73 i|.l R-3..... 101 8,3 I ............. ' I ' ' J' ‘ I I I I . . . I I I ' ' I ' ' ' ' I ' ' ‘ ' I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' ' ' ‘ I ' ' mZz-> 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #64355:2-Hexanol, 2-methyl- _5b------------------------------------------------------------------

7.40 7.60 7.80 8.00 5000- m/z 58.05 19.34%

nZz-> <\bundance , 20 31 | 1, — I -53||| 30 40 45

50 60 70 80 90 #7666: Acetic acid, cyano-, 1.1-dimethylethyl ester 5b___________________ 101

100 110 120 130

^7.40 - 7,60 —7:80—8.00 -m/z-“- 41.05' L 7t57% 5000 41

68 U.......... J I.............................................. 126 Ti/z-> 20 30 40 50 6o’ 70 ro 90 '' ioo ' i-io'' 120 no ■7.40 7.60 7.80 8.00

23837.D NP103001.M Thu Nov 01 13:28:40 2001 Page 2

NYC-WTC_M0d89342

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NYC-WTC_000089342Source: NYC Law Department, mirrored locally

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