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GCMS analysis results for sample AE02788, March 11, 2002

Machine-extracted title · confidence 100%

Laboratory report for DEP sample AE02788 showing unknown compounds and surrogate recovery data from March 11, 2002.

NYC-WTC_000005584–000005594

Folder label: “GCMS X 2/6/02 A 3/1/02

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Scanned page image, NYC-WTC_000005591
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NYC 9/11 Public Portal Document Library search compound Report

Data File C:\HPCHEM\l\DATA\MAR0102\2788 .D Vial: 22 Acq On 2 Mar 2002 5:00 am Operator: Sample gc/ms scan 2/6 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 1 2-Methyl-5-hexen-3-ol Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

8.20 0.30 ug/1 25103 1,4-Dichlorobenzene-d4 12.31

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Methyl-5-hexen-3-ol 114 C7H140 032815-70-6 9 2 Formamide, N/N-dimethyl- 73 C3H7NO 000068-12-2 5 3 1-Butanamine, 3-methyl- 87 C5H13N 000107-85-7 4 4 1-Butanamine, 2-methyl- 87 C5H13N 000096-15-1 4 Abundance C Scan 344 (8.199 min): 2788.D (-) m/ z 73. 0.0 100.00% 3

5000 43

55 69. 7.80 8.00 8.20 8.40 8.60 . ......... ........ 39111,1149, THTPT - 87 1 m/z 11 “ " I " " 1 ‘1 ■' I " " I 42.95 26.70% m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #3017:2-Methyl-5-hexen-3-ol 73

5000-

27 43 55 — 7.80__ 8.00 ; m/z M. 4 0.95 8.20 8.40 11.70% 8.60

31 । 1" I " " l" ■' i" ' ‘ i' r" J 11111'1111" 11" 111" 1' ‘11 “ " I " "70 ' 81 I " " I " ITT’ ■ 111111111111111 m/Z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance . 44 73

7.80 8.00 8.20 8.40 8.60 5000 m/z 44.95 10.60% 30 15 27 3841 58 " ' ‘ l " " I ■' " i " " i " “ i " " i ■ ■ " i" " I' " ' i " " i " " i" " 1" " I " " I " " I" " 11" 11" " I " m/z-> . 5. 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #62884:1-Butanamine, 3-methyl- ........ .......... ' I ■ ' ' ' I ' ' ‘ ' I ' ' ' ' I ‘ ‘ ‘ ' I ' ' 30 7.80 8.00 8.20 8.40 8.60 i m/z 71.00 8.34% 5000

27 4144 55 5Q 70 — 87 ....... 11...... TTTWWWTRTTTTTTTHT >i 111111'। |।। 11! ।' | > ■ j' ।" mr 111111111111111 nvz-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 7.80 8.00 8.20 8.40 8.60

2788.D GCMS0208.M Tue Mar 05 10:53:36 2002 Page 1

NYC-WTC_000005591

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NYC-WTC_000005591Source: NYC Law Department, mirrored locally

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