GCMS analysis results for sample AE02788, March 11, 2002

NYC 9/11 Public Portal Document ulprary earcn compound Keporc

Data File C:\HPCHEM\1\DATA\MAR0102\2788.D Vial: 22 Acq On 2 Mar 2002 5:00 am Operator: Sample gc/ms scan 2/6 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 2 Anthracene-dlO- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

25.85 0.25 ug/1 29557 Phenanthrene-dl0 25.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-du.0- • 4 188 C14D10 001719-06-8 86 2 Phenanthrene -d10y / 188 C14D10 001517-22-2 86 3 Cyclohexanone, phenylhydrazone 188 C12H16N2 000946-82-7 9 4 1,4-Naphthalenedione, 2-hydroxy-3-m 188 C11H803 000483-55-6 9 Abundance Scan 2267 (25.853 min); 2788.D (-) . m/z 188.10 100.00% / 188 1 1

5000 ....... ............ 78 44 ‘' I' *'' 111' * I m/z->.......... 40.... 50 60 66 — 70 80 94 160

90 100 110 120 130 140 150 160 170 180 190 mL IIT — i 25.60 25.80 26.00 26.20 m/z 18 .05 19.86% Abundance #19957: Anthracene-d 10- 188

5000- 25.60 25.80 26.00 26.20 . 8° 94I 160 m/z 77.95 17.30% DO WIIWTT)WTPIPTITTT ......................... *' i ■ ■ ■ ■ । ■ ■ ■ ■ । | ■11 ■1 ■ -1 * * ■ ■ i1111111 ri । "T’ 1 r*1 nVz-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance .. 188 - 25.60 25.80 26.00 26.20 5000 m/z 184.. 10 15.88% 80 94

.. 1... 160 66 9 m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19927: Cyclohexanone, phenylhydrazone ■ ■ i ■ ■ 188 25.60 25.80 26.00 26.20 93 m/z 16 . 05 12.84% 5000- 65 77 106 ...... ............. 145 | 159 no |i I 120 132 " I " " I' ' “ i'' ■ i “ " i “ -- —0—1————- 2ur m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 25.60 25.80 26.00 26.20

2788.D GCMS0208.M Tue Mar 05 10:53:40 2002 Page 2

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