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GCMS analysis results for sample AE04025, Mar 15 2002

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Laboratory report documenting GCMS analysis of sample AE04025 conducted on March 15, 2002.

NYC-WTC_000038314–000038323

Folder label: “GCMS X 2/22/02 A 2/24/02

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Scanned page image, NYC-WTC_000038322
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NYC 9/11 Public Portal Document „ Library searcn compound Keporc

Data File : C:\HPCHEM\1\DATA\FEB2102\4025.D Vial: 80 Acq On : 25 Feb 2002 12:43 am Operator: Sample : gc/ms scan 2/22 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 2 Anthracene-dlO- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

25.88 0.24 ug/1 21914 Phenanthrene-dl0 25.73

Hit# of 5 > Tentative ID MW MolForm CAS# Qual

1 Anthracene-diO- 66 188 C14D10 001719-06-8 38 2 Phenanthrene-diO 188 C14D10 001517-22-2 9 3 5-Methy'l-2-phenyl-2-hexenal 188 C13H160 021834-92-4 9 4 Antipyrine 188 C11H12N2O 000060-80-0 9 Abundance / Scan 2270 (25.878 min): 4025.D (-) m/z 188.10 100.00% 108

5000

94 66 156 25.60 25.80 26.00 26.20 । 80 —11I111111

L i 11E m/z 189.05 24.78% m/Z—2 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19957: Anthracene-d10- 188

5000 25.60 25.80 26.00 26.20 80 m/z 93.90 20.60% | 66 94 160 — | —— 1 ! 1 I ' ■ l......... ..... — .il miz-> 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #1 995.8: Phenanthrene-d10 i 188 --- — 25.60 25.80 26.00 26.20 5000 m/ Z 65.95 13.83%

160 66 8|° 94 ................................ —................. |j.; ■ i ■ ' ■ ■ i ' 1 ’ ■ i ' • ■ ■ I ■ ■ ■ I , m/z--> 60 7G 80 90 100 110 120 130 140 150 160 170 180 190 ■Abundance #69187: 5-Methyl-2-phenyl-2-hexenal ' 'T'-1 • ■ I • 1 • 188 25.60 25.80 26.00 26.20 | 117 m/z 187.15 13.66%

5000 104 132 145 173 ,______ — — — 1 miz-> 60 70 80 90 100 110 120 130 140 150 160 170 180 190 25.60 25.80 26.00 26.20

4025.D GCMS0208.M Wed Mar 13 11:40:09 2002 Page 2

NYC-WTC_000038322

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NYC-WTC_000038322Source: NYC Law Department, mirrored locally

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