GCMS blank analysis report for sample AE12735, June 2002

NYC 9/11 Public Portal Document Llorary searcn compound Keporc

Data File C:\MSDCHEM\1\DATA\0 6 0 7 0 2\LBA.D Vial: 10 Acq On 7 Jun 2002 3:55 pm Operator: Sample gc/ms scan 6/3 Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\060302.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 15 Phenanthrene-dlO Concentration Rank 12 R.T. EstConc Area Relative to ISTD R.T. 23.06 0.31 ug/L 328576 Phenanthranene-dl0 22.91 Hit# of 5 Tentative ID MW MolForm CAS# Qual A

1 Phenanthrene-diO 188 C14D10 001517-22-2 72 y/ 2 Anthracene-dlO- 188 C14D10 001719-06-8 64* 3 Antipyrine 188 C11H12N2O 000060-80-0 25 4 Antipyrine 188 C11H12N2O 000060-80-0 9 Abundance Scan 3401 (23.062 min): LBA.D (-3395) (-) m/z 188.10 100.00% 188

5000

80 94 22.80 23.00 23.20 23.40 0 mpmp-H 43 57 66 11.1l..111700070.732.,11150 ... m/z 189.10 25.35% m/z-> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 Abundance #79827: Phenanthrene-d1 0 188

- 5000 22.80 23.00 23.20 23.40 80 m/z 94.10 19.84% 94 160 30 42 52 108118 132 146 66 11 rI, 170179.1,1 0 120]—WPTNTTHTTTHttTTtn n/z-> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 Abundance #79826: Anthracene-d10- 188

22.80 23.00 23.20 23.40 5000 m/z 80.10 15.26%

17 30 42 52 66 80 94 160 t . 0- ■ I' “ 1 !■' ■ ' I'' " 11 “ ‘ I11' '1111 ■ 11'1 H 11 ■ !| +198 118.132.14617017— iz-> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 — Abundance #79725: Antipyrine 188 22.80 23.00 23.20 23.40 96 m/z 187.10 11.81% 5000 77 56 105 27 39 67 nl 130 145 159 173 ii I. 115 mmm+ 0 ' i ■' ■' i' m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 22.80 23.00 23.20 23.40

LBA.D 060302.M Mon Jun 10 11:27:42 2002 Page 18

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