GCMS analysis results for sample AE11283, May 2002

NYC 9/11 Public Portal Document Llorary searcn compound Keporc

Data File : C:\MSDCHEM\1\DATA\020516\11283.D Vial: 11 Acq On : 16 May 2002 7:15 pm Operator: Nefliu Sample : sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 Peak Number 3 Phenanthrene-diO Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 31.96 0.33 ug/1 23641 Phenanthrene-dl0 31.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Phenanthrene-d10 188 C14D10 001517-22-2 59 2 Phosphonic acid, (3-methyl-3-pen... 188 C8H13O3P 022152-34-7 53 3 Pentaycyclo [7.3.1.1. (4,12) .0 (2,7) . . . 188 C14H20 1000215-61-8 38 4 Anthracene-diO- 188 C14D10 001719-06-8 17 Abundance Scan 4915 (31.958 min): 11283. D (-4906) (-) m/ z 188.10 100.00% 188

5000 /................ 80 31.60 31.80 32.00 32.20 44 •' । Iiip...... 156 | 1 ' i ' ■ ■ ■ i ' 1 k 426 m/z 80.10 28.24% Tl/Z-> 50 100 150 200 250 300 350 400 Abundance #79827: Phenanthrene-d10 188

5000 m 31.60 31.80 32.00 32.20 m/z 189.30 26.45% 80 160 30,57,4,4.190, 132,4. ,1 ■n/z-> 50 100 150 200 250 300 350 400 Abundance #79704: Phosphonic acid, (3-methyl-3-penten-1-ynyl)-, dime... 188

31 60 31.80 32.00 32.20 5000 77 m/z 184.10 21.95% 35 109 155 . .1281 I ll. I n/z-> 50 100 150 200 250 300 350 400 Abundance #79715: Pentacyclo[7.3.1.1 .(4,12).0(2,7).0(6,11 )tetradeca... ' I ' ' ' 1 1 1 1 1 'V 1 1 1 I ' 188 31.60 31.80 32.00 32.20 m/Z 78.10 17.50% 5000 91 55 131 159 111 i 1 ’ kA 4 i , h, I , ■ . I T ■ , Ffr , ,-T |-| I I IT r I I I | I n/z—> 50 100 150 200 250 300 350 400 31.60 31.80 32.00 32.20

11283.D SCAN020507.M Fri May 17 13:03:27 2002 Page 5

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