GCMS analysis results, sample AE12324, June 2002

NYC 9/11 Public Portal Document Llorary searen compound Keporc Data File : C:\MSDCHEM\1\DATA\052902\12324.D Vial: 12 f Acq On : 29 May 2002 7:03 pm Operator: McLean Sample : gc/ms scan 5/24 fb Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 17 Phenanthrene, 9-methyl- Concentration Rank 16 R.T. EstConc Area Relative to ISTD R.T. 22.54 0.28 ug/L 287114 Phenanthranene-dl0 22.91 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Phenanthrene, 9-methyl- 192 C15H12 000883-20-5 2 1,5-Naphthalenedithiole 192 C10H8S2 1000223-69-5 38 3 Phenanthrene, 1-methyl- 192 C15H12 000832-69-9 36 4 Anthracene, 9-methyl- 192 C15H12 000779-02-2 36 Abundance Scan 3311 (22.533 min): 12324.D (-3304) (-) m/z 192.10 00.00% 192

5000 , .... 7 k.... / I 96 146 160 22.20 22.40 22.60 22.80

n/z—> 42 55 70 82 118 O 11111 (1111 [ 111 ij i i‘7i 11111.111 > 11111,111 11 > i —mp 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 km H m/z 191.00 18.91% Abundance #81033: Phenanthrene, 9-methyl- 192

(). 5000 22.20 22.40 22.60 22.80 m/z 96.00 16.15% . 29 39 51 63 74 83. T 115 126 139 152 165 176 | O*/11BnaaBanqanaspeanaq3mc))* ri i rHi M’l । Pl r| 11111 in 11 j 11111»» j'| 1111 pi 11j । j rhptt ■ ■ i" niz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #80950:1,5-Naphthalenedithiole 192 TI 22.20 22.40 22.60 22.80 5000 m/z 193.10 15.22 115 128 159 40 57 69 79 96 147 — . 1 . . | ■ 11lr . ■ , ill', ! , f‘177 ||| 0 1 i “ • The • i • * miz-> 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 200 Abundance #125856: Phenanthrene, 1-methyl- ■ • i ■ ■ ' ‘ i ■ ■ i ■ ■ ■ ' i ■ ■ • ‘ I 19/2 22.20 22.40 22.60 22.80 m/z 146.10 14.71%| 5000

96

n/z—> 27 39 51 63 82 ,| ODTmmmmmmmtmtH 115 126 139 152 165 178 । 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 k a 22.20 22.40 22.60 22.80 • i * ‘ M k i

12324.D 052202.M Mon Jun 03 10:52:27 2002 Page 20

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