GCMS analysis results, sample AE12533, June 2002

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Data File : C:\MSDCHEM\l\DATA\052902\12533.D Vial: 24 Acq On : 30 May 2002 4:49 am Operator: McLean Sample : gc/ms scan 5/28 Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library- : C:\DATABASE\NIST98.L

Peak Number 16 Phenanthrene, 9-methyl- Concentration Rank 16 R.T. EstConc Area Relative to ISTD R.T. 22.54 0.27 ug/L 316769 Phenanthranene-dl0 22.91 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Phenanthrene, 9-methyl- 192 C15H12 000883-20-5 59 / 2 Anthracene, 9-methyl- 192 C15H12 000779-02-2 45 1 3 Phenanthrene, 1-methyl- 192 C15H12 000832-69-9 45 ' 4 Phenanthrene, 2-methyl- 192 C15H12 002531-84-2 45 v Abundance Scan 3311 (22.533 min): 12533.D (-3305) (-) m/z 192.10 100.00%! 192

5000

118 82 96 146 160 | 22.20 22.40 22.60 22.80

■ntz~> 42 52 70 -mmmll++7 0- 11 “'11 “ “ 1111111 “111 mH atyilspoo -H 2030405060 70 8090 100 110120 130140 150160 170 180190 200 m/z 191.10 17.37%| Abundance #81033: Phenanthrene, 9-methyl- 192

5000 22.20 22.40 22.60 22.80 m/ z 146.00 13.11%| _ 96 165 । 1 ft 115i j 1126 83 illJ t j 11' 11 Tlt 29 39 51 63 74 iglrth 0 »{414 41«41 f 11 j 4 4 0 4 4 * । i’ri 111 139 152 lt 176 . 11 j j't 1 r ‘| 1111 |*l 7 ri j ?! 11 j 1 rht । 11111 rt’ j “i" m/z-> 2030405060 70 8090 100 110120 130140 150160 170 180 190 200 Abundance #125849: Anthracene, 9-methyl- 192 A 1 22.20 22.40 22.60 22.80 5000 m/z 193.10 12.93%|

96 165 28 39 51 63 74 83 . I,l 105 115 126 139 152 tl 176 , 0: 11 M Mg .. 1'|>... fi,. . 11'1,, 1. IT. (′ n it rri’i 11! I 1111 mer "T‘ 1111 i'i'i 11 ( rHt 11 ill miz-> 2030405060 70 8090 100 110 120 130 140 150 160 170 180 W 200 Abundance #125856: Phenanthrene, 1-methyl- 1 1 i • ' • • i • ‘ i ‘ ■ ■ ■ i ‘ • i 192 22.20 22.40 22.60 22.80 m/z 82.10 11.14%| 5000

98 P 27 39 51 63 82 j 115 126 139 152 190 178 , | - 0 »j» j 141111 > ।: t«t jj j j 11 i'i 111 j rt * [* rtt j 1’ ’ I j j i j । ti1! 11111111 j r’r i r j 11’| ■ i j 11 'prl r j i rit j t r’rj’tt i j 11 r m/z—> 2030405060 70 8090 100110 120 130 140 150 160 170 180 190 200 22.20 22.40 22.60 22.80

12533.D 052202.M Mon Jun 03 11:45:41 2002 Page 19

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