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GCMS sample analysis results, AE11903, June 3, 2002

Machine-extracted title · confidence 100%

Laboratory report presenting analytical results for target compounds and surrogate recovery data for water sample AE11903.

NYC-WTC_000012908–000012936

Folder label: “GCMS X 5-21-02 A 5-22-02

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Scanned page image, NYC-WTC_000012927
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NYC 9/11 Public Portal Document Library Search Compound Report. Data File : C:\MSDCHEM\1\DATA\052202\11903.D Vial: 10 Acq On : 22 May 2002 9:09 pm Operator: Mclean Sample : 5/21 ad Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L Peak Number 12 Phenanthrene, 1-methyl- Concentration Rank 19 R.T. EstConc Area Relative to ISTD R.T. 22.54 0.29 ug/L 326488 Phenanthranene - dl 0 22.91 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Phenanthrene, 1-methyl- 192 C15H12 000832-69 2 Phenanthrene , 9-methyl- 192 C15H12 000883-20 3 Phenanthrene, 2-methyl- 192 C15H12 002531- 4 Bitoscanate 192 C8H4N2S2 004044- Abundance Scan 3312 (22.539 min): 11903.D (-3304) (-) m/z 192.10 192

5000

82 96 146 160

rnfe-> 0 mmmmhmptto 42 51 70 ] ,l 118 mTp hmmmnor 20 30 40 50 60 70 80 90 100 110 120130 140 150 160 170 180 190 200 4 22.20 22.40 22.60 22.80 m/z 191.10 17.49% Abundance #125856: Phenanthrene, 1-methyl- 192

5000 22.20 22.40 22.60 22.80 m/z 146.10 17.12% 98 27 39 51 63 82 , 115 126 139 152 165 178 0 11111111111-| 11 > i pi 1111 fl > rj । "ti Drft i TPWTTTTTTTTTTTTTPTTTTTNTTHDTl gor miz-> 2030405060 70 8090 100 110 120 130 140 150 160 170 180 190 200 Abundance #81033: Phenanthrene, 9-methyl- 192 A 22.20 22.40 22.60 22.80 5000 m/z 193.10 16.28%

96

n/z-> 29 39 51 63 74 83 TPPgnpHt iMJ rl 1111 r 0 'i । n n 11J j rj rt i j PTi FI’i 11 i‘ri r’i rfl 115 126 139 152 165 176 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 JL Abundance #125842: Phenanthrene, 2-methyl- 192 22.20 22.40 22.60 22.80 m/z 96.10 12.04% 5000

96 27 39 51 63 82 J 115 126 139 152 165 176 0 1111111 > n i*| n 1114 i'i । i'i 11 TMtr "h /I i'| 111 rpri 11, inj ii.i-j i1ii pl i n । i'i1, 111 rlt । i I’l tugor 14 I 1 1 1 1 1 1 1 i ■ • • ■ i ■ ■ ■ ■ i tnfz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 22.20 22.40 22.60 22.80

11903.D 052202.M Tue May 28 12:07:51 2002 Page 15

NYC-WTC_000012927

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