GCMS analysis results, sample AE09967, May 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\MSDCHEM\1\DATA\050602\9967.D Vial: 23 Acq On 7 May 2002 5:37 am Operator: Mclean Sample 4/25 Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 7 Phenanthrene, 2-methyl- Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

22.58 0.34 ug/L 380344 Phenanthranene-dl0 22.96

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Phenanthrene, 2-methyl- 192 C15H12 002531-84-2 50 2 Phenanthrene, 1-methyl- 192 C15H12 000832-69-9 50 3 Phenanthrene, 9-methyl- 192 C15H12 000883-20-5 50 4 1,5-Naphthalenedithiole 192 C10H8S2 1000223/69-5 45 Abundance Scan 3319 (22.580 min): 9967.D (-3312) (-) m/z 192.10100.00% 192

5000 ...................... /............... / 1 i ■ 1 1 1 i 1 1 1 1 i 1 1 1 1 i ■ ■ ■ 1 i 1 146 160 mlz-> 41 49 118 TTTTTHTT 70 , — on | , . J, 96 I I I I I I I I t I I I'l I I I I I I I I I I I I I I I I I I I I I I I I I I I I I > I 111111 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 m 22.20 22.40 22.60 22.80 23.00 m/Z 191.10 19.44%

Abundance #125842: Phenanthrene, 2-methyl- 192

5000 22.20 22.40 22.60 22.80 23.00 m/z 146.10 15.17% 96

mlz-> 27 39 51 63 TI—Ium—n—muT 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 82 I 115 126 139 152 195 176 1*rl i'11' i1" ' i11'11' " 11'' ■ ‘‘i ■1'11'1 ■ " i'''11111111 +U Abundance #125856: Phenanthrene, 1-methyl- 192 1..... . 22.20 22.40 22.60 22.80 23.00 5000 m/z 193.10 13.61%

96 PE mfe-> 27 ————51— ———39 63 821 115 126 11E1*51111011111119110E1000000TNTTT 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 139 152 20 178 + Abundance #81033: Phenanthrene, 9-methyl- 192 22.20 22.40 22.60 22.80 23.00 m/z 96.00 13.17%

5000-

96 165

/z—> 29 39 51 63 74 83 II 115 126 139 152 + 176 1 I " " I ‘ 1 1 1 I 1 1 1 1 I' 1 1 ' I ' I ' "Ti 1* rl I 11sy*assp—ni 1711 I I | I I I i‘| I I I I ]■! I I I | 111 rl 11 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 aplapr ■ । । । ■ 1 ■ । 1 1 ' r । ' 22.20 22.40 22.60 22.80 23.00

9967.D 050102.M Tue May 07 15:45:31 2002 Page 11

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