GCMS analysis results, sample AE09967, May 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\MSDCHEM\1\DATA\050602\9967.D Vial : 23 Acq On 7 May 2002 5:37 am Operator: Mclean Sample 4/25 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 8 Phenanthrene-diO Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

23.11 0.64 ug/L 707191 Phenanthranene-dl0 22.96

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Phenanthrene-diO 188 C14D10 001517-22-2 90 2 Anthracene-dlO- 188 C14D10 001719-06-8 90 3 3-Amino-4-methyl-6-methoxyquinoline 188 C11H12N2O 1000213-71-3 40 4 Cycloheptanone, 4-phenyl- 188 C13H160 067688-28-2 40 Abundance Scan 3409 (23.109 min): 9967. D (-3403) (-) m/z 188.15 100.00% 188

5000 ........ / 80 94 ■ ■ i > । ■ i ■ ■ 1 ' I ' 1 ' 1 I 43 57 71 J . . 160 I 22.80 23.00 23.20 23.40 ........ .. 146 ........... 111 i"111 i । r i i r i re । । i i । i^i । i’| I I Ji । i i I i ]‘i i H | । ! I r j'l r TT t r i i | Ti I i | i I । I | I I i I | I i i i | I | I l | I I I I | I TT F[ f n m/ Z 94.10 16.66% m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79827: Phenanthrene-d10 188

5000 ........ /........................ 1’111 11,417* I + 22.80 23.00 23.20 23.40 m/z 189.15 14.31% 80 94 160 30 42 52 66 m/z-> 11 I I I I I I I I I I I I I I I I 1 I I I I I I I I I I I I I j

10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 ,, I'l | 108 118 132 146 111 I ] I 11 11 I r i i [ ITTTTT r । । | H i 11 i 11 11179179ll, TT

Abundance #79826: Anthracene-d10- 188 ----------------- 22.80 23.00 23.20 23.40 5000 m/z 184.10 14.12%

RA 80 94 160 , , 17 30 42 52 66 J | | i ' i T| i r i > p i i i i [ I i i t । I I i i । J I I i j I | I I | I .1 108 118 132 ' 146 1.7179179/,.. I 11 11 11 I 11 IIII [ I I I I [ I I I I I I TT /z-> 10 20 30 40 50 60 70 80 90 100 110120 130 140 150 160 170 180 190 Abundance #79771:3-Amino-4-methyl-6-methoxyquinoline 188 22.80 23.00 23.20 23.40 m/ z 80.10 11.82% 145 5000

117

m/z-> Ti I'1111 41 51 63

10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 77 89 102 130 TT I 159 173 I ... ,............. 22.80 23.00 23.20 23.40

9967.D 050102 .M Tue May 07 15:45:31 2002 Page 12

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