GCMS analysis results for sample AE11930, June 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\DATA\052302\11930.D Vial: 10 Acq On : 23 May 2002 5:18 pm Operator: Mclean Sample : 5/22ad Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C: \DATABASE\NIST98 . L ********************************************************************* Peak Number 13 Phenanthrene-diO Concentration Rank 13

R.T. EstConc Area Relative to ISTD R.T. 23.07 0.28 ug/L 244946 Phenanthranene-dl0 22.91 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Phenanthrene-diO 188 C14D10 001517-22-2 64 2 Anthracene-dlO- 188 C14D10 001719-06-8 64 3 3-Amino-4-methyl -6-methoxyquinoline 188 C11H12N2O 1000213-71-3 40 4 Antipyrine 188 C11H12N2O 000060-80-0 40 Abundance Scan 3402 (23.068 min): 11930.D (-3395) (-) m/z 188.15 100.00% 188

5000

94 22.80 23.00 23.20 23.40 52 66 20, mTTHT o- IITMTTTTT 160 m/ z 94.10 21.55% m/z-> 10 20 30 40 50 60 70 80 90 100110120 130 140 150 160 170 180 190 Abundance #79827: Phenanthrene-d10 188

5000 22.80 23.00 23.20 23.40 80 m/z 189.10 14.74% 94 160 30 42 52 66 11 108118 132 146 ,|. 1701791 0 E2——m0mm0—mHnhnmutTTTT mlz-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190 Abundance #79826: Anthracene-d10- 188

22.80 23.00 23.20 23.40 5000 m/z 80.10 11.50%

rr 80 94 160 , , 17 30 42 52 66 108118 132 146 1i 170179 0'Te]mmHghtt TIT‘T 4 iz-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190 Abundance #79771:3-Amino-4-methyl-6-methoxyquinoline V.......................... ‘ * i■’•1i11■■ । ‘ ‘ 1 । ■ ‘ 188 22.80 23.00 23.20 23.40 m/z 184.10 10.62% 145 5000

41 51 63 77 89 102 117 130 0 TFTTTTp-------t*p----t mm 1 159 173 I 1 n/z-> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 22.80 23.00 23.20 23.40

11930.D 052202.M Wed May 29 09:50:21 2002 Page 16

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