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GCMS analysis results sample AE11926, June 2002

Machine-extracted title · confidence 90%

Laboratory report documenting GCMS analysis of sample AE11926 conducted on June 4, 2002, including surrogate recovery data.

NYC-WTC_000013454–000013475

Folder label: “GCMS X 5/22/02 A 5/23/02”

←Page 21 of 22→
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\l\DATA\052302\11926.D Vial: 6 Acq On : 23 May 2002 2:02 pm Operator: Mclean Sample : 5/22ad Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 13 Phenanthrene-dlO Concentration Rank 12 R.T. EstConc Area Relative to ISTD R.T. 23.07 0.27 ug/L 287291 Phenanthranene-dl0 22.91

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Phenanthrene-dlO 188 C14D10 001517-22-2 93 2 Anthracene-dlO- 188 C14D10 001719-06-8 93 3 3-Amino-4-methyl-6-methoxyquinoline 188 C11H12N2O 1000213-71-3 42 4 4-Methyl-2-(4-fluorophenyl)pyrim... 188 C11H9FN2 076128-67-1 40 Abundance Scan 3402 (23.068 min): 11926.D (-3396) (-) m/z 188.10 100.00% US

5000

80 94 160 22.80 23.00 23.20 23.40 43 57 66 0 —ampmmHtr ll m/ Z 189.10 18.88% • i ■ “ ■ i' ‘ “ i ■ ‘ ■ • i “ ■ ■ i ■ ■ ’ ’14 i" • ■ i mz-> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 Abundance #79827: Phenanthrene-d10 us

5000 22.80 23.00 23.20 23.40 80 m/z 94.10 15.39% 94 160 30 42 52 66 0-I—901——03m9mm——u—m—uHnntt 11 108118 132 146 I 170179.1,1 I ’T miz-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190 Abundance #79826: Anthracene-d10- 188 ' 22.80 23.00 23.20 23.40 5000 m/z 80.10 14.03%

„ 80 94 160 । 0- 17 30 42 52 P J J 108118 132 146 .U 170179/ TT—r miz-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190 Abundance #79771:3-Amino-4-methyl-6-methoxyquinoline US 22.80 23.00 23.20 ‘23,40 m/z 184.10 11.94% 145 5000

41 51 63 77 89 102 117 130 159 173 ,i 0 | । । ' | 11 I । | ■ I 11 |'ll. rlr rlllm | , i’ll . ! r’lel rrlr ■ ri rI l l rt . ■ rrlll | ■ ritl ■ ■ ■ r . . | . rrl ■ . T’I n/z-> 10 2030405060 70 8090 100110120130140150160 170 180 190 22.80 23.00 23.20 23.40

11926.D 052202.M Wed May 29 09:47:52 2002 Page 16

NYC-WTC_000013474

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NYC-WTC_000013474Source: NYC Law Department, mirrored locally

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