GCMS analysis results sample AE11926, June 2002

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Laboratory report documenting GCMS analysis of sample AE11926 conducted on June 4, 2002, including surrogate recovery data.

NYC-WTC_000013454–000013475

Folder label: “GCMS X 5/22/02 A 5/23/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\l\DATA\052302\11926.D Vial: 6 Acq On : 23 May 2002 2:02 pm Operator: Mclean Sample : 5/22ad Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 12 Phenanthrene, 9-methyl- Concentration Rank 11 R.T. EstConc Area Relative to ISTD R.T. 22.54 0.27 ug/L 289121 Phenanthranene-dl0 22.91 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Phenanthrene, 9-methyl- 192 C15H12 000883-20-5 59 2 Phenanthrene, 1-methyl- 192 C15H12 000832-69-9 59 3 Thiocyanic acid, 2-benzothiazoly... 192 C8H4N2S2 006011-99-0 59 4 Phenanthrene, 2-methyl-192 C15H12 002531-84-2 59 Abundance Scan 3312 (22.539 min): 11926.D (-3301) (-) m/z 192.10 100.00% 192

5000

96 146 160 | 22.20 22.40 22.60 22.80 66 82 TIWTITTTITTTTTTTTTHTTHT ripaal.pirorp-n12RP.rry0al1y0Aham21.211/0a11/am1] Wp 42 m/z 191.10 16.78% 0- m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #81033: Phenanthrene, 9-methyl- 192

5000- T L 22.20 22.40 22.60 22.80 1*‘‘I

m/z 146.10 15.32% 29 39 51 63 74 83 J 115 126 139 152 165 176 | 0 11PTTmmmprht “ I “ miz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #125856: Phenanthrene, 1-methyl- 1912

22.20 22.40 2260 22.80 5000 m/z 193.00 11.95%

miz-> 27 39 51 63 82 l 0 TETuuum—mam—ntpap——hm7 TPmTTTTTTTTTTH

Abundance 96 115 126 139 152 100 178 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 #80870: Thiocyanic acid, 2-benzothiazolyl ester IRK u .......... 2. 1912 22.20 22.40 22.60 22.80 m/z 96.00 10.91

5000

45 90 108 122 134 148 160 I..... 0- mHp 111 Ji 11'| 111 > 11111 [ ■ ■ 11111. I'i 111 <. i. ।111 > 111111111 i‘l 11111111111 “ ■ i ■1 ■ ■ i ■ • ■ ■ । ■1 । • • • • । ■ ■ • > । n/z—> 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 200 22.20 22.40 22.60 22.80

11926.D 052202.M Wed May 29 09:47:52 2002 Page 15

NYC-WTC_000013473

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