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GCMS analysis report sample AE09677, May 23, 2002

Machine-extracted title · confidence 95%

GCMS laboratory report for sample AE09677 detecting unknown compounds and 2,4-DDD on May 23, 2002.

NYC-WTC_000013154–000013183

Folder label: “GCMS X 5/21/02 A 5/21/02

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Scanned page image, NYC-WTC_000013174
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\l\DATA\052102\9677.D Vial: 15 Acq On : 22 May 2002 12:44 am Operator: Mclean Sample : re-extract Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C: \DATABASE\NIST98 . L Peak Number 12 Phenanthrene, 9-methyl- Concentration Rank 17 R.T. EstConc Area Relative to ISTD R.T. 22.54 0.29 ug/L 309598 Phenanthranene-dl0 22.91 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Phenanthrene, 9-methyl- 192 C15H12 000883-20-5 45 2 5H-Dibenzo[a,d]cycloheptene 192 C15H12 000256-81-5 42 3 Thiocyanic acid, 2-benzothiazoly ... 192 C8H4N2S2 006011-99-0 42 4 Phenanthrene, 2-methyl- 192 C15H12 002531-84-2 42 Abundance Scan 3312 (22.539 min): 9677.D (-3289) (-) m/z 192.10 100.00% 192

5000

. 96 146 160 A m/z-> 42 70 82 .1 118 0 mmmthup —HH-pr . j... 11। 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 mmL 22.20 22.40 22.60 22.80 m/z 191.10 17.02% Abundance #81033: Phenanthrene, 9-methyl- 192

5000 T 22.20 22.40 22.60 22.80 m/z 146.10 15.92% 96 165 । i 29 39 51 63 74 83 l 115 126 139 152 ,| 176 0 TIWWTPTPTTTTTTTTTTTTTTTTITTTTTTTTT“ । ■1 m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #80999:5H-Dibenzo[a,d]cycloheptene 192 .. 10A • I • /• * • I 22.20 22.40 22.60 22.80 177 5000 m/z 96.00 14.23% 89 165 39 51 76 I „ 1 14 I 63 102 115 128 139 152 0 mpMpmmmmmpmm ‘‘111 iz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #80870: Thiocyanic acid, 2-benzothiazolyl ester *‘1***I‘* i 1 ' ' 1 i 1 ' ' I 192 22.20 22.40 22.60 22.80 m/z 193.10 14.06% 5000

69 o 108 134

m/z—> 45 1..A2.9244112 0-'h 11" 11'111111'' 111 " I' i i । 148 160 ppm ’ •' I •k • ■1 ■ ■ ■

20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 L ■ ■ i ■ ■ ■ ■ i ■ ■ I ‘ 22.20 22.40 22.60 22.80 ’ ‘ I ’ 1 ‘ ‘ I

9677.D 052202.M Wed May 22 11:34:26 2002 Page 15

NYC-WTC_000013174

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NYC-WTC_000013174Source: NYC Law Department, mirrored locally

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