GCMS analysis report sample AE09677, May 23, 2002

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Library Search Compound Report

Data File : C:\MSDCHEM\l\DATA\052102\9677.D vial: 15 Acq On : 22 May 2002 12:44 am Operator: Mclean Sample : re-extract Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 13 Phenanthrene-diO Concentration Rank 18

R.T. EstConc Area Relative to ISTD R.T.

23.07 0.27 ug/L 287110 Phenanthranene-dl0 22.91

Hit# of 5 Tentative ID MW MolForm CAS# . Qual, A 1 Phenanthrene-diO 188 C14D10 001517-22-2 90)V) 2 Anthracene-dlO- 188 C14D10 001719-06-8 86< 4 3 Pentacyclo[7.3.1.1. (4,12) .0 (2,7) ... 188 C14H20 1000215-61-8 59 4 Naphthalene, 1,7-dimethoxy- 188 C12H1202 005309-18-2 42 Abundance Scan 3402 (23.068 min): 9677. D (-3395) (-) m/z 188.10 100.00% 188

5000

80 94 158 43 57 66 .... 22.80 23.00 23.20 23.40 0 —MOmPPTTTTTTTTTTmpTTTH m/ z 80.10 18.08% m/z-> 10 20 30 40 50 60 70 80 90 100110120 130140150160170180190 Abundance #79827: Phenanthrene-d10 188

5000 22.80 23.00 23.20 23.40 m/z 94.00 16.44% 80 94 160 30 42 52 66 l| .108118 132 146 II, 170179 0 TIWWTIWTTTTTTHTTH II n p ii 11 1 H t u |l 1 1 TWTNTTTTTTTTTTDT n/z-> 10 2030405060 70 8090 100110120130140150160170180190 Abundance #79826: Anthracene-d10- 188 — 22.80 23.00 23.20 23.40 5000 m/z 189.10 16.19%

80 94 160 66 । ■ 11111 17 30 42 52 0-TTTTTTTTTT -H+ *1108118 132 146 ,|| 170179|.i w- n/z-> 10 2030405060 70 8090 100110120 130140150160170180190 ) Abundance #79715: Pentacyclo|7.3.1.1.(4,12).0(2,7).0(6,11)]tetradeca... L 188 22.80 23.00 23.20 23.40 m/z 184.10 13.18%

5000 79 91 55 67 105 117 145 159 m/z—> 0- l I ‘1 “ 1 ‘1 “ I , 170 । 173 mmmmm 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 22.80 23.00 23.20 23.40

9677.D 052202.M Wed May 22 11:34:27 2002 Page 16

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