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GCMS blank analysis results sample AE11926, May 2002

Machine-extracted title · confidence 90%

Quality control document showing GCMS blank results for multiple volatile organic compounds analyzed on May 29, 2002.

NYC-WTC_000013418–000013443

Folder label: “GCMS X 5/22/02 A 5/23/02

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Scanned page image, NYC-WTC_000013436
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\l\DATA\052302\522LB.D Vial: 3 Acq On : 23 May 2002 11:36 am Operator: Mclean Sample : 5/22ad Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan ' * Library : C: \DATABASE\NIST98 . L ********************************************************************* Peak Number 12 Phenanthrene-diO Concentration Rank 16

R.T. EstConc Area Relative to ISTD R.T.

23.07 0.24 ug/L 188670 Phenanthranene-dl0 22.91

Hit# Of 5 Tentative ID MW MolForm CAS# Qual A 1 Phenanthrene-diO 188 C14D10 001517-22-2 874 2 Anthracene-dlO- 188 C14D10 001719-06-8 86> 3 3-Amino-4-methyl-6-methoxyquinoline 188 C11H12N2O 1000213-71-3 40 4 Naphthalene, 1,7-dimethoxy- 188 C12H1202 005309-18-2 40 Abundance Scan 3402 (23.068 min): 522LB.D (-3396) (-) m/z 188.10 100.00% 188

5000 .............................. ........... .. 80 94 44 57 66 , 160 22.80 23.00 23.20 23.40 0- 11'" i m/z 80.10 17.11% n/z-> 10 20 30 40 50 60 70 80 90 100110120 130 140 150 160 170 180 190 Abundance #79827: Phenanthrene-d10 188

5000 22.80 23.00 23.20 23.40 80 m/z 94.10 16.95% 94 160 30 42 52 66 , 11 108118 132 146 H. 170179/ 0 TIITTTTTTHTTH 1 ‘I n/z-> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160170 180 190 Abundance #79826: Anthracene-d10- 188

22.80 23.00 23.20 23.40 5000 m/z 184.10 16.36%

80 94 160 | 0 17 ° . [ ,11111111 42 52 j 11111111111111 30 111111111111 108118 132 146 I. 170179] 111 in 11111111111111 > 111 it|'> 111111 ■ । rl’l’l T m/z-> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 Abundance #79771:3-Amino-4-methyl-6-methoxyquinoline 1(8 22.80 23.00 23.20 23.40 m/z 189.10 16.28% 145 5000

63 77 89 117 ‘1 130 159 41 51 102 0-pmmp n/z—> 10 2030405060 70 8090 100110120130140150160170180190 22.80 23.00 23.20 23.40

522LB.D 052202.M Wed May 29 09:38:59 2002 Page 15

NYC-WTC_000013436

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NYC-WTC_000013436Source: NYC Law Department, mirrored locally

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