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GCMS analysis results, sample AE12534, June 2002

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Laboratory report showing GCMS analysis results for sample AE12534 including surrogate recovery data on June 10, 2002.

NYC-WTC_000014578–000014606

Folder label: “GCMS X 5/28/02 A 5/29/02

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\l\DATA\052902\12534.D Vial: 25 Acq On : 30 May 2002 5:37 am Operator: McLean Sample : gc/ms scan 5/28 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 13 Phenanthrene-diO Concentration Rank 19

R.T. EstConc Area Relative to ISTD R.T.

23.06 0.31 ug/L 301464 Phenanthranene-dl0 22.91

Hit# of 5 Tentative ID MW MolForm CAS# Qua

1 Phenanthrene-diO 188 C14D10 001517-22-2 86 2 Anthracene-dlO- 188 C14D10 001719-06-8 86 3 Benzene, 1-(1-cyclohexen-l-yl)-4... 188 C13H160 020758-60-5 45 4 3-Amino-4-methyl-6-methoxyquinoline 188 C11H12N2O 1000213-71-3 45 Abundance Scan 3401 (23.062 min): 12534.D (-3395) (-) m/z 188.10 100.00% 188

5000

40 51 66 80 94 160 22.80 23.00 23.20 23.40 0 TWTH 110—10000110"T1"11"73 1’1"HH4 m/z 189.10 15.40% mlz-> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 Abundance #79827: Phenanthrene-d10 1(18

5000 22.80 23.00 23.20 23.40 80 94 m/z 94.10 13.64% 160 30 42 52 66 , 0TIWTIWTTITTTTHTTHTT1 I 108118 132 146 11, 179179/1 miz-> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 Abundance #79826: Anthracene-d10- 1(18 . 22.80 23.00 23.20 23.40 5000 m/z 184.10 11.99%

66 80 94 160 17 30 42 52 0 TITmBBIm—m—mp—uumphv4+10811812.146—179179.. miz-> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 Abundance #79791: Benzene, 1-(1-cycfohexen-1-yl)-4-methoxy- 1(8 22.80 23.00 23.20 23.40 m/z 187.10 - 11.92% 5000 160

115 129 145 173

m/z—> 0 41 51 65 77 — 102 Xu - TTpt TTur 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 T y Tri 22.80 23.00 23.20 23.40

12534.D 052202.M Mon Jun 03 11:46:48 2002 Page 16

NYC-WTC_000014598

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