GC/MS analysis results, sample AE10850, May 14 2002

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Laboratory report page showing GC/MS analysis for sample AE10850 including surrogate recovery data on May 14, 2002.

NYC-WTC_000023531–000023546

Folder label: “GCMS X 5/9/02 A 5/13/02”

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\l\DATA\051302\10850.D Vial: 15 Acq On : 13 May 2002 10:55 pm Operator: Mclean Sample : 5/9 kb Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 7 Phenanthrene-diO Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

23.11 0.40 ug/L 410008 Phenanthranene-dl0 22.95

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Phenanthrene-diO 188 C14D10 001517-22-2 59 2 Anthracene-d10- 188 C14D10 001719-06-8 47- 3 3-Amino-4-methyl-6-methoxyquinoline 188 C11H12N2O 1000213-71-3 40 4 Antipyrine 188 C11H12N2O 000060-80-0 40 Abundance Scan 3409 (23.109 min): 10850.D (-3402) (-) m/z 188.10 100.00% US

5000

94 43 ,57 66 80 158 I i 22.80 23.00 23.20 23.40 0 mOTWTTPTTTTTTTRTTTTTT '1111' i1'111111111'111 mr ■ 11 > j 1111111 fl ।" " । m/z 94.05 19.15% m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79827: Phenanthrene-d10 188

5000 .. A........ 22.80 23.00 23.20 23.40 m/z 189.10 18.14% 80 94 160 30 42 52 66 mlz-> 0 1 ■" 11 ■ 11 ■ I ■ । 11 11 108118 132 146 1111111111 -1 “ I'1111111TTp-rt-r 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 7.04179179,,. Abundance #79826: Anthracene-d10- --------- 22.80 23.00 23.20 23.40 5000 m/z 184.05 13.91% A RA 80 94 160 , , 17 30 42 52 00 , | 108 118 132 146—++,..... 0 v mlz-> 10 20 30 40 50 60 70 80 90 .100110 120 130 140 150 160 170 180 190 Abundance #79771:3-Amino-4-methyl-6-methoxyquinoline ............. .... US 22.80 23.00 23.20 23.40 m/z 80.10 10.11% 145 5000

m/z~> 0 L r ... I | 41 51 63 77 89 102 117 130 i 159 173 | , ‘n rll1 rililr ! . ilt i l r‘‘r . , "I’t- ! | ! rill- l ■ r!‘11 . ------ 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 II . /y... 22.80 23.00 23.20 23.40

10850.D 050102.M Tue May 14 11:44:44 2002 Page 10

NYC-WTC_000023545

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NYC-WTC_000023545Source: NYC Law Department, mirrored locally

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GCMS analysis results for sample AE10896, May 21 2002 · Box DEP Box 18

NYC-WTC_000024083

Laboratory report detailing GCMS analysis of sample AE10896 conducted on May 21, 2002, including surrogate recovery data.

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