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GC/MS analysis results, sample AE10850, May 14 2002

Machine-extracted title · confidence 100%

Laboratory report page showing GC/MS analysis for sample AE10850 including surrogate recovery data on May 14, 2002.

NYC-WTC_000023531–000023546

Folder label: “GCMS X 5/9/02 A 5/13/02

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Scanned page image, NYC-WTC_000023544
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NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\DATA\051302\10850.D Vial: 15 Acq On : 13 May 2002 10:55 pm Operator: Mclean Sample : 5/9 kb Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 6 2-Propenal, 3-(3,4-dimethox... Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T.

22.58 0.27 ug/L 282022 Phenanthranene-dl0 22.95

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propenal, 3-(3,4-dimethoxyphen... 192 C11H1203 004497-40-9 40 2 1H-2-Indenone,2,4,5,6,7,7a-hexah... 192 C13H20O 1000196-69-5 40 3 Anthracene, 2-methyl- 192 C15H12 000613-12-7 36 4 Phenanthrene, 3-methyl- 192 C15H12 000832-71-3 36 Abundance Scan 3319 (22.580 min): 1 0850. D (-3310) (-) m/z 192.10 100.00% 192

5000 ........ ,..... . - ,

m/z-> 42 _ 82 96 70 । | 120 146 160 0! TTTTTTTTTTTTPTPTTTTT || 10 20 30 40 50 60 70 80 90 100110120130140150160 170180190 200 Ju 22.20 22.40 22.60 22.80 23.00 m/z 191.00 17.36% Abundance #80953:2-Propenal, 3-(3,4-dimethoxyphenyl)- 192 161

5000 1 1 1 ‘ ' 1 I ' ' J......IL 22 20 22.40 22.60 22.80 23.00 77 121 149 177 m/z 193.10 15.77% 52 91 103 138

m/z-> 0 ' ■ i" " r1" i" " i " " i11 r " 'T ‘ MHLL 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200 HT Abundance #80945:1 H-2-lndenone,2,4,5,6,7,7a-hexahydro-3-(1-methylet... 192 149 ■ i ■ ■ ' ■ i 1 ■ 1 1 1 1 ' ‘ ' 1 1 22.20 22.40 22.60 22.80 23.00 177 5000 m/z 96.00 13.07% 41 93 107 121 135 164 55 67 79 1+4 Al + +1 HA 4++447++ + 27 .......... IOUII 0 1,1 —0170 I’T m/z-> 10 20 30 40 50 60 70 80 90 100110120 130140150160170180190 200 Abundance #81034: Anthracene, 2-methyl- 1-p-. - 7 r Tit I ■ ' 7 ' I ’ 192 22.20 22.40 22.60 22.80 23.00 m/z 146.00 12.58% A 5000

82 ge 165 18 27 39 51 69 || 115 126 139 152 .1 176 0 —TMTTTTTTTTTTTTTmTtTHThTt 4-rrrrr ,................. .4. /z-> 10 20 30 40 50 60 70 80 90 100110120130140 150160 170180190 200 22.20 22.40 22.60 22.80 23.00

10850.D 050102.M Tue May 14 11:44:42 2002 Page 9

NYC-WTC_000023544

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NYC-WTC_000023544Source: NYC Law Department, mirrored locally

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