GCMS sample analysis results for AE10604, May 10 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File C:\MSDCHEM\1\DATA\050702\10604.D Vial: 9 Acq On 7 May 2002 7:39 pm Operator: Mclean Sample 5/3 kb Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 6 2-Propenal, 3 -(3,4-dimethox. . . Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

22.58 0.32 ug/L 392744 Phenanthranene- dl 0 22.96

Hit# of 5 Tentative ID MW MolForm CAS# Qual

l 2-Propenal, 3-(3,4-dimethoxyphen... 192 C11H1203 004497-40-9 45 2 Anthracene, 9-methyl- 192 C15H12 000779-02-2 42/ 3 1,5-Naphthalenedithiole 192 C10H8S2 1000223-69-5 38 4 2-Imidazolidinone, 1-methoxy-3-p... 192 C10H12N2O2 052420-43-6 /38 Abundance Scan 3319 (22.580 min): 10604.D (-3312) (-) “m/z 192.10 100.00% 192 ft

5000

82 96 ■ i 1 ■ L 111Bt r T | > ‘ i | >

54 66 . , 146 1 60I 22.20 22.40 22.60 22.80 23.00 42 00 120 I1.......... .. ■ | L1 I I I I I I J I I I I I I ■ r । ! I . ■ । , 11............ ............................ pi l.............. ................. - m/Z 191.10 19.59% mlz-> 20 30 40 50 60 70 80 90 100110 120130 140150 160 170 180 190 200 Abundance #80953: 2-Propenal, 3-(3,4-dimethoxyphenyl)- 192 161

5000 TT । 22.20 22.40 22.60 22.80 23.00 77 91 121 149 177 m/ z 96.10 15.83% 52 64 103

/z-> ........................ ,...... .11,,, n । । । । । । । । ,,1... 11 .....,..... — 1 rn'111 ■ ■ I ■ ■ I I I I I I I I I I > j I I I I I I I I I I I I I I I I

20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 1.. X4.. .... 1 Abundance #125848: Anthracene, 9-methyl- 192 ■ I ' 1 ' ' I 1 I ' 1 ' ' I ' 22.20 22.40 22.60 22.80 23.00 5000 m/z 146.10 12.50%

96 27 39 51 63 82 .1 115 126 139 152 165 176 „ TLWOTTIUTPTTTTTTTI H I ' ['''r I " "'l111 rli 1 111’4" . 1111 - P II I /z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #80950:1,5-Naphthalenedithiole .................... /..............._ 1 I ' 1 1 ' I ' ' 1 1 I ■ ■ ' 1 I ' l 1 I I > 192 22.20 22.40 22.60 22.80 23.00 m/z 193.00 12.40%

5000 115 128 159 147 I 40 57 69 79 .................... \ m/z-> ----- 177 hill 36,198,1. —L TT " 1 [1 ।111 ■ । ' 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 22.20 22.40 22.60 22.80 23.00 "kiT

10604.D 050102.M Thu May 09 09:08:25 2002 Page 9

NYC-WTC_000045608