GCMS sample analysis results for AE10604, May 10 2002

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Laboratory report detailing GC/MS analysis of sample AE10604 including surrogate recovery data in May 2002.

NYC-WTC_000045595–000045617

Folder label: “GCMS X 5/3/02 A 5/7/02”

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File C:\MSDCHEM\1\DATA\050702\10604.D Vial : 9 Acq On 7 May 2002 7:39 pm Operator: Mclean Sample 5/3 kb Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 7 Anthracene-dlO- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

23.11 0.46 ug/L 567558 Phenanthranene-dl0 22.96

Hit# of 5 Tentative ID MW MolForm CAS# Qual .

1 Anthracene-dlO- 188 C14D10 001719-06-8 91 D/7 2 Phenanthrene-diO 188 C14D10 001517-22-2 87 Z 3 2-Quinolinecarboxaldehyde, 8-hyd... 188 C10H8N2O2 005603-22-5 40 4 -(4-Tolyl)-3-methyl-pyrazol-5-one 188 C11H12N2O 035496-19-6 38 Abundance Scan 3409 (23.109 min): 10604.D (-3402) (-) m/z 188.10 100.00% 188

5000

— 80 94 160 22.80 23.00 23.20 23.40 43 52 66............... 132 1?......... |,„ m/z 94.05 14.64% TT I ■ ■'11 r'111111 " i111111'111111 ‘ i11111'1 " i1 ‘11 r' ■1 r 1' ■ r 111 r '1 ' r " 11'111 11I m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79826: Anthracene-d10- 188

i > । । — । y । ।l—i । । । । । । । । । । । । 5000 22.80 23.00 23.20 23.40 m/z 189.10 14.15% 80 94 160 , , 66 v146—4179179. 17 30 42 52 11111111111 11 ■ ■ ■ 111 ■ 11 108 118’ 132 11111 ‘ i1" ' I" " 111 " i11' I i i । mri [■! rr t । I r i m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79827: Phenanthrene-d10 188 1 ! I I I I I y I I I I I I I I I I _I I 1 I"

22.80 23.00 23.20 23.40 5000 m/z 80.05 10.63%

80 94 160 30 42 52 66 । । ii < । । । । ।।।>।i । | I । । । । I H।।iI I। । | 108 118 132 + 11111 | l lT| PI I I | I 1 I l | t I T T | I'll 146 TT 179179. trrrr

m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #125696: 2-Quinolinecarboxaldehyde, 8-hydroxy-, oxime ‘ /‘‘‘/T‘11111177114‘‘‘I 188 22.80 23.00 23.20 23.40 m/z 184.05 9.78%

5000 143 89 115 51 64 76 | 102 I, 15 170 /z-> 130 ' r 111 r " 111111 r 1 ■' 1'" 1' i ’l 1 ‘...... 'I |'11, |i‘*111111. । - 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 / 11 1111 । 11 । 11 11 । ! । i H 22.80 23.00 23.20 23.40

10604.D 050102.M Thu May 09 09:08:29 2002 Page 10

NYC-WTC_000045609

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NYC-WTC_000045609Source: NYC Law Department, mirrored locally

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GCMS analysis results for sample AE10609, May 10 2002 · Box DEP Box 25

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Laboratory report detailing GC/MS analysis of sample AE10609 including surrogate recovery data in May 2002.

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