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GCMS analysis results for sample AE11381, May 22 2002

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Laboratory report showing GCMS analysis results for sample AE11381 conducted on May 22, 2002.

NYC-WTC_000025102–000025126

Folder label: “GCMS X 5/15/02 A 5/17/02

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NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\DATA\051702\11380.D Vial: 7 Acq On : 17 May 2002 5:40 pm Operator: Mclean Sample : 5/15 ad Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 8 Anthracene-dlO- Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T. 23.11 0.49 ug/L 608625 Phenanthranene-dl0 22.95 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-diO- 188 C14D10 001719-06-8 80 2 Phenanthrene-diO 188 C14D10 001517-22-2 72 3 2-Quinolinecarboxaldehyde, 8-hyd. . . 188 C10H8N2O2 005603-22-5 40 4 3-Amino-4-methyl-6-methoxyquinoline 188 C11H12N2O 1000213-71-3 38 Abundance Scan 3409 (23.109 min): 11380. D (-3402) (-) m/z 188.10 100.00% 188

5000

80 94 158 22.80 23.00 23.20 23.40

mz-> OTWTPTTT)T 43 57 66 H । | 207 ’ I ! | I t | I I i I | I T I+ I I11 | [I1 I | | I I 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 r " ■ r1111" " r1" i" i" " i" " i1" m/z 80.05 A 19.98% Abundance #79826: Anthracene-d10- 188

5000 22.80 23.00 23.20 23.40 m/z 94.05 16.55% p 80 94 160 17 30 42 52 66 , J 108118 132 146 1 170 0 ' r "11" " 11 111111111111 [ 11111111111 T——1—0nu———Tt——TTT -ryn-r /z-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 Abundance #79827: Phenanthrene-d10 188 /I 22.80 23.00 23.20 23.40 5000 m/z 189.20 15.52%

80 94 160 30 1 ■ 42 52 66.j■. l,l | n । 11 108118 132 146 II 170 J 0 TID0071’ 1111 ■ 111111111 TTTTTTTTTTTTTTTTTTTTTTTTTTT Trnr m/z-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 Abundance #125696: 2-Quinolinecarboxaldehyde, 8-hydroxy-, oxime 188 22.80 23.00 23.20 23.40 m/z 184.10 13.36%

5000 143 51 64 76 89 102 115 130 , . 158 170 n/z-> 0 ' i' ■111 i"1' i ■ I1" 1 r " 11 10 20 30 40 50 60 70 80 90 100110120130140150160170180190 200 210 4—HHHH ..................................................... 22.80 23.00 23.20 23.40

11380.D 050102.M Mon May 20 15:46:52 2002 Page 11

NYC-WTC_000025120

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NYC-WTC_000025120Source: NYC Law Department, mirrored locally

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