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GCMS analysis results for sample AE12475, June 2002

Machine-extracted title · confidence 100%

Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE12475 conducted on June 4, 2002.

NYC-WTC_000014125–000014146

Folder label: “GCMS X 5/24/02 A 5/28/02

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\l\DATA\052802\12475.D Vial: 13 Acq On : 29 May 2002 12:04 am Operator: McLean Sample : 5/24 ad Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e ?.* Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L Peak Number 13 Anthracene -dlO- Concentration Rank 10 R.T. EstConc Area Relative to ISTD R.T. 23.07 0.31 ug/L 304187 Phenanthranene-dl0 22.91 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Anthracene-diO- 188 C14D10 001719-06-8 90 2 Phenanthrene-diO 188 C14D10 001517-22-2 87 - 3 2-Quinolinecarboxaldehyde, 8-hyd... 188 C10H8N2O2 005603-22-5 40 4 3-Amino-4-methyl -6-methoxyquinoline 188 C11H12N2O 1000213-71-3 38 Abundance Scan 3402 (23.068 min): 12475.D (-3393) (-) m/z 188.10 100.00% 188

5000

80 94 43 54 66 158 22.80 23.00 23,20 23.40

niz-> 0 111111111 j. । > i j >‘l 11 j. 1111 > 1111111. 11 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 p 1’148 m/z 94.00 21.90% Abundance #79826: Anthracene-d10- 188

5000 22.80 23.00 23.20 23.40 m/ z 80.00 17.00%| 17 30 42 52 80 94 J 108118 132 146 I 170179|,i | 160 0- 11.... 11... |.!.. 11, II111111 il 11111111111 rtlli r|ll 1111111111II111111111-111 > ’hyun 111 " 1111111 n/z-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190 Abundance। #79827: Phenanthrene-d10 1118

22.80 23.00 23.20 23.40 5000 m/z 189.10 16.93%

80 94 160 30 42 52 66 I I ,H| 1 1 I lj ,|Hl I | I I108118 132 146> 170179,1,1 0-'i । । । । i । । H । । । । । । ।i।>।।II।।।iIH। ............................................. . . . . . TTTTTTTPTTT I I | I 1 I I | II I I | Il l || I I I I |

10 2030405060 70 8090 100 110 120 130 140 150 160 170 180 190 Abundance #125696:2-Quinolinecarboxaldehyde, 8-hydroxy-, oxime 188 22.80 23.00 23.20 23.40 m/z 184.00 : 9.99 5000-

143 51 64 76 89102 1 130 158 170 0 - 10 20 30 40 50 60 70 80 90 100110120130140150160170180190 palpar.... ' 22.80 23.00 23.20 23.40

12475.D 052202.M Thu May 30 10:43:34 2002 Page 16

NYC-WTC_000014145

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NYC-WTC_000014145Source: NYC Law Department, mirrored locally

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